methyl N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycinate

Base Information

Chemical Name:methyl N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycinate
CAS No.:1314097-19-2
Molecular Formula:C₂₉H₄₅N₅O₈
Molecular Weight:591.705
Hs Code.:

Synonyms:methyl N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycinate

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Chemical Property of methyl N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycinate

Chemical Property:

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Technology Process of methyl N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycinate

There total 4 articles about methyl N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1314097-12-5
N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycine

: 39687-95-1
isocyanoacetic acid methyl ester

: 110-58-7
n-Pentylamine

: 1314097-19-2
methyl N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycinate

Guidance literature:: In methanol; at 80 ℃; for 0.05h; Microwave irradiation; Sealed tube;
DOI:10.1016/j.tet.2018.10.018

Reference yield:

: 110-58-7
n-Pentylamine

: 1314097-19-2
methyl N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycinate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium sulfate / 0.08 h / 45 °C / sealed tube; Microwave irradiation; neat (no solvent)

2: water; lithium hydroxide / tetrahydrofuran / 0.05 h / 60 °C / sealed tube; Microwave irradiation

3: sodium sulfate / 0.08 h / 45 °C / sealed tube; Microwave irradiation; neat (no solvent)

With water; sodium sulfate; lithium hydroxide; In tetrahydrofuran; 1: Ugi reaction / 3: Ugi reaction;
DOI:10.1039/c1ob05471f

Reference yield:

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 1314097-19-2
methyl N-N-(((benzyloxy)carbonyl)glycyl)-N-pentylglycylglycyl-N-pentylglycylglycinate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium sulfate / 0.08 h / 45 °C / sealed tube; Microwave irradiation; neat (no solvent)

2: water; lithium hydroxide / tetrahydrofuran / 0.05 h / 60 °C / sealed tube; Microwave irradiation

3: sodium sulfate / 0.08 h / 45 °C / sealed tube; Microwave irradiation; neat (no solvent)

With water; sodium sulfate; lithium hydroxide; In tetrahydrofuran; 1: Ugi reaction / 3: Ugi reaction;
DOI:10.1039/c1ob05471f