N-decyl-3,5-bis(1-([1,1'-biphenyl]-4-yl)-1H-1,2,3-triazol-4-yl)benzamide

Base Information

Chemical Name:N-decyl-3,5-bis(1-([1,1'-biphenyl]-4-yl)-1H-1,2,3-triazol-4-yl)benzamide
CAS No.:1417405-97-0
Molecular Formula:C₄₅H₄₅N₇O
Molecular Weight:699.899
Hs Code.:

Synonyms:N-decyl-3,5-bis(1-([1,1'-biphenyl]-4-yl)-1H-1,2,3-triazol-4-yl)benzamide

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Chemical Property of N-decyl-3,5-bis(1-([1,1'-biphenyl]-4-yl)-1H-1,2,3-triazol-4-yl)benzamide

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Technology Process of N-decyl-3,5-bis(1-([1,1'-biphenyl]-4-yl)-1H-1,2,3-triazol-4-yl)benzamide

There total 5 articles about N-decyl-3,5-bis(1-([1,1'-biphenyl]-4-yl)-1H-1,2,3-triazol-4-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1417406-00-8
N-decyl-3,5-diethynylbenzamide

: 31656-91-4
4-azidobiphenyl

: 1417405-97-0
N-decyl-3,5-bis(1-([1,1'-biphenyl]-4-yl)-1H-1,2,3-triazol-4-yl)benzamide

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper; In dichloromethane; water; for 72h; Inert atmosphere;
DOI:10.1039/c2ob26797g

Reference yield:

: 618-58-6
3,5-dibromobenzoic acid

: 1417405-97-0
N-decyl-3,5-bis(1-([1,1'-biphenyl]-4-yl)-1H-1,2,3-triazol-4-yl)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 70 °C / Inert atmosphere

3.1: potassium carbonate / tetrahydrofuran; methanol / 3 h

4.1: copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper / dichloromethane; water / 72 h / Inert atmosphere

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; 2.1: |Sonogashira Cross-Coupling / 4.1: |Huisgen Cycloaddition;
DOI:10.1039/c2ob26797g

Reference yield:

: 1417405-99-2
N-decyl-3,5-bis(2-(trimethylsilyl)ethynyl)benzamide

: 1417405-97-0
N-decyl-3,5-bis(1-([1,1'-biphenyl]-4-yl)-1H-1,2,3-triazol-4-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrahydrofuran; methanol / 3 h

2: copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper / dichloromethane; water / 72 h / Inert atmosphere

With copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; water; 2: |Huisgen Cycloaddition;
DOI:10.1039/c2ob26797g