tert-butyl {3-[(4-methoxy-2,6-dimethylphenyl)sulfonyl]propoxy}dimethylsilane

Base Information

Chemical Name:tert-butyl {3-[(4-methoxy-2,6-dimethylphenyl)sulfonyl]propoxy}dimethylsilane
CAS No.:959640-92-7
Molecular Formula:C₁₈H₃₂O₄SSi
Molecular Weight:372.601
Hs Code.:

Synonyms:tert-butyl {3-[(4-methoxy-2,6-dimethylphenyl)sulfonyl]propoxy}dimethylsilane

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Chemical Property of tert-butyl {3-[(4-methoxy-2,6-dimethylphenyl)sulfonyl]propoxy}dimethylsilane

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Technology Process of tert-butyl {3-[(4-methoxy-2,6-dimethylphenyl)sulfonyl]propoxy}dimethylsilane

There total 2 articles about tert-butyl {3-[(4-methoxy-2,6-dimethylphenyl)sulfonyl]propoxy}dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 959640-91-6
tert-butyl {3-[(4-methoxy-2,6-dimethylphenyl)thio]propoxy}dimethylsilane

: 959640-92-7
tert-butyl {3-[(4-methoxy-2,6-dimethylphenyl)sulfonyl]propoxy}dimethylsilane

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 16h;

Reference yield:

: 701-69-9
4-methoxy-2,6-dimethylbenzenethiol

: 959640-92-7
tert-butyl {3-[(4-methoxy-2,6-dimethylphenyl)sulfonyl]propoxy}dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.33 h / 0 °C

1.2: 16 h / 20 °C

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 0 - 20 °C

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 959640-92-7
tert-butyl {3-[(4-methoxy-2,6-dimethylphenyl)sulfonyl]propoxy}dimethylsilane

: 74-88-4
methyl iodide

: 3-[(4-methoxy-2,6-dimethylphenyl)sulfonyl]propan-1-ol

: 959640-93-8
3-[(4-methoxy-2,6-dimethylphenyl)sulfonyl]butan-1-ol

Guidance literature:: tert-butyl {3-[(4-methoxy-2,6-dimethylphenyl)sulfonyl]propoxy}dimethylsilane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

methyl iodide; In tetrahydrofuran; hexane; at -78 - 20 ℃;

With ammonium chloride; In tetrahydrofuran; hexane; water;