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C14H9BrFNO2S

Base Information
  • Chemical Name:C14H9BrFNO2S
  • CAS No.:1589004-60-3
  • Molecular Formula:C14H9BrFNO2S
  • Molecular Weight:354.199
  • Hs Code.:
C<sub>14</sub>H<sub>9</sub>BrFNO<sub>2</sub>S

Synonyms:C14H9BrFNO2S

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Chemical Property of C14H9BrFNO2S
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Technology Process of C14H9BrFNO2S

There total 1 articles about C14H9BrFNO2S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
5-bromo-6-fluoro-1H-indole; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;
benzenesulfonyl chloride; In tetrahydrofuran; at 0 - 25 ℃; for 6h;
Guidance literature:
C14H9BrFNO2S; tributyl(1-ethoxyvinyl)stannane; With tetrakis(triphenylphosphine) palladium(0); lithium chloride; In 1,4-dioxane; Inert atmosphere; Reflux;
With hydrogenchloride; In 1,4-dioxane; water;
Guidance literature:
Multi-step reaction with 2 steps
1: lithium chloride; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane / Inert atmosphere; Reflux
2: titanium(IV) isopropylate / toluene / Reflux
With titanium(IV) isopropylate; tetrakis(triphenylphosphine) palladium(0); lithium chloride; In 1,4-dioxane; toluene;
upstream raw materials:

5-bromo-6-fluoro-1H-indole

benzenesulfonyl chloride

Downstream raw materials:

C20H23FN2O3S2

C16H12FNO3S

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