N-benzoyl-N-[9-(2,2-dimethyl-6-phenethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl]-benzamide

Base Information

• Chemical Name: N-benzoyl-N-[9-(2,2-dimethyl-6-phenethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl]-benzamide
• CAS No.: 859731-93-4
• Molecular Formula: C₃₄H₃₁N₅O₅
• Molecular Weight: 589.651

Synonyms:N-benzoyl-N-[9-(2,2-dimethyl-6-phenethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl]-benzamide

Chemical Property of N-benzoyl-N-[9-(2,2-dimethyl-6-phenethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl]-benzamide

Chemical Property:

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Technology Process of N-benzoyl-N-[9-(2,2-dimethyl-6-phenethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl]-benzamide

There total 3 articles about N-benzoyl-N-[9-(2,2-dimethyl-6-phenethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzoyl-N-[9-(2,2-dimethyl-6-styryl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl]-benzamide (595608-13-2) → N-benzoyl-N-[9-(2,2-dimethyl-6-phenethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl]-benzamide (859731-93-4)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 4h;

DOI:10.1016/j.bmcl.2005.03.107

Reference yield:

benzyltriphenylphosphonium chloride (1100-88-5) → N-benzoyl-N-[9-(2,2-dimethyl-6-phenethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl]-benzamide (859731-93-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 46 percent / sodium bis(trimethylsilyl)amide / tetrahydrofuran / 3 h / 55 °C

2: H₂ / Pd/C / ethyl acetate / 4 h

With hydrogen; sodium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate; 1: Wittig reaction;

DOI:10.1016/j.bmcl.2005.03.107

Reference yield:

N6,N6-bis-benzoyl-2',3'-O-isopropylideneadenosine-5'-aldehyde (119244-47-2) → N-benzoyl-N-[9-(2,2-dimethyl-6-phenethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl]-benzamide (859731-93-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 46 percent / sodium bis(trimethylsilyl)amide / tetrahydrofuran / 3 h / 55 °C

2: H₂ / Pd/C / ethyl acetate / 4 h

With hydrogen; sodium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate; 1: Wittig reaction;

DOI:10.1016/j.bmcl.2005.03.107

upstream raw materials:

N-benzoyl-N-[9-(2,2-dimethyl-6-styryl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-yl]-benzamide

benzyltriphenylphosphonium chloride

N⁶,N⁶-bis-benzoyl-2',3'-O-isopropylideneadenosine-5'-aldehyde

Downstream raw materials:

9-((3aR,4R,6R,6aR)-2,2-Dimethyl-6-phenethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-yl)-9H-purin-6-ylamine

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