methyl 2-acetamido-5-(4-nitro-3-(2-methoxy-2-oxoethyl)-phenoxy)benzoate

Base Information

Chemical Name:methyl 2-acetamido-5-(4-nitro-3-(2-methoxy-2-oxoethyl)-phenoxy)benzoate
CAS No.:1192318-96-9
Molecular Formula:C₁₉H₁₈N₂O₈
Molecular Weight:402.361
Hs Code.:

Synonyms:methyl 2-acetamido-5-(4-nitro-3-(2-methoxy-2-oxoethyl)-phenoxy)benzoate

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Chemical Property of methyl 2-acetamido-5-(4-nitro-3-(2-methoxy-2-oxoethyl)-phenoxy)benzoate

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Technology Process of methyl 2-acetamido-5-(4-nitro-3-(2-methoxy-2-oxoethyl)-phenoxy)benzoate

There total 3 articles about methyl 2-acetamido-5-(4-nitro-3-(2-methoxy-2-oxoethyl)-phenoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29640-99-1
methyl 2-(5-fluoro-2-nitrophenyl)acetate

: 154664-44-5
2-acetylamino-5-hydroxybenzoic acid methyl ester

: 1192318-96-9
methyl 2-acetamido-5-(4-nitro-3-(2-methoxy-2-oxoethyl)-phenoxy)benzoate

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In dimethyl sulfoxide; at 20 ℃; for 72h;

Reference yield:

: 350-46-9,178603-76-4
4-Fluoronitrobenzene

: 1192318-96-9
methyl 2-acetamido-5-(4-nitro-3-(2-methoxy-2-oxoethyl)-phenoxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / DMF (N,N-dimethylformamide) / -5 °C

2: 18-crown-6 ether; potassium carbonate / dimethyl sulfoxide / 72 h / 20 °C

With 18-crown-6 ether; potassium tert-butylate; potassium carbonate; In DMF (N,N-dimethylformamide); dimethyl sulfoxide;

Reference yield:

: 394-31-0
2-amino-5-hydroxybenzoic acid

: 1192318-96-9
methyl 2-acetamido-5-(4-nitro-3-(2-methoxy-2-oxoethyl)-phenoxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 0.67 h / 140 °C

1.2: 20 °C

2.1: 18-crown-6 ether; potassium carbonate / dimethyl sulfoxide / 72 h / 20 °C

With 18-crown-6 ether; potassium carbonate; In dimethyl sulfoxide;