O,O,O-triacetylisocybrodol

Base Information

• Chemical Name: O,O,O-triacetylisocybrodol
• CAS No.: 75225-93-3
• Molecular Formula: C₂₁H₂₈O₆
• Molecular Weight: 376.45

Synonyms:O,O,O-triacetylisocybrodol

Chemical Property of O,O,O-triacetylisocybrodol

Chemical Property:

Purity/Quality:

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Technology Process of O,O,O-triacetylisocybrodol

There total 12 articles about O,O,O-triacetylisocybrodol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

acetic anhydride (108-24-7) + isocybrodol (75225-87-5) → O,O,O-triacetylisocybrodol (75225-93-3)

Guidance literature:

With pyridine; In dichloromethane; for 6h; Heating;

DOI:10.1139/v81-310

Reference yield: 97.0%

tetraethylammonium acetate (1185-59-7) + 3-((3-(2-acetoxyethyl)-6-bromomethyl-2,4-dimethyl)phenyl)-2-methyl-(Z)-2-propenyl bromide (79801-70-0) → O,O,O-triacetylisocybrodol (75225-93-3)

Guidance literature:

In acetone; for 1h; Heating;

DOI:10.1139/v81-311

Reference yield: 78.0%

acetic anhydride (108-24-7) + isocybrodol methyl ether (79801-66-4) → Acetic acid 4-(2-acetoxy-ethyl)-2-((Z)-3-acetoxy-2-methyl-propenyl)-3,5-dimethyl-benzyl ester (75225-90-0,75225-93-3)

Guidance literature:

With iron(III) chloride; for 18h; Ambient temperature;

DOI:10.1139/v81-311

upstream raw materials:

tetraethylammonium acetate

3-((3-(2-acetoxyethyl)-6-bromomethyl-2,4-dimethyl)phenyl)-2-methyl-(Z)-2-propenyl bromide

acetic anhydride

isocybrodol

Downstream raw materials:

6-<2-(4-nitrophenylseleno)ethyl>-5,7-dimethylphthalide

isocybrodol

cybrodol

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