isocybrodol methyl ether

Base Information

Chemical Name:isocybrodol methyl ether
CAS No.:79801-66-4
Molecular Formula:C₁₆H₂₄O₃
Molecular Weight:264.365
Hs Code.:

Synonyms:isocybrodol methyl ether

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Chemical Property of isocybrodol methyl ether

Chemical Property:

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Technology Process of isocybrodol methyl ether

There total 6 articles about isocybrodol methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74973-56-1
2-(4-methoxymethyl-2,6-dimethylphenyl)ethanol

: 79801-66-4
isocybrodol methyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: bromine / nitromethane / 0.5 h / 0 °C

2: 95 percent / pyridinium tosylate / CH₂Cl₂ / 1 h / Ambient temperature

3: 25 percent / 1.6 M n-butyllithium / tetrahydrofuran / 1.) -78 deg C, 1 h; 2.) RT, 5 h

4: 152 mg / 0.3 M aq. H₂SO₄ / acetone / 7 h / Heating

With n-butyllithium; sulfuric acid; bromine; pyridinium p-toluenesulfonate; In tetrahydrofuran; nitromethane; dichloromethane; acetone;
DOI:10.1139/v81-311

Reference yield:

: 79801-57-3
2-(3-bromo-4-methoxymethyl-2,6-dimethylphenyl)ethanol

: 79801-66-4
isocybrodol methyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / pyridinium tosylate / CH₂Cl₂ / 1 h / Ambient temperature

2: 25 percent / 1.6 M n-butyllithium / tetrahydrofuran / 1.) -78 deg C, 1 h; 2.) RT, 5 h

3: 152 mg / 0.3 M aq. H₂SO₄ / acetone / 7 h / Heating

With n-butyllithium; sulfuric acid; pyridinium p-toluenesulfonate; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1139/v81-311

Reference yield:

: 74973-57-2
1-bromo-3(2-(tetrahydro-2H-pyran-2-yl)oxyethyl)-6-methoxymethyl-2,4-dimethylbenzene

: 79801-66-4
isocybrodol methyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 25 percent / 1.6 M n-butyllithium / tetrahydrofuran / 1.) -78 deg C, 1 h; 2.) RT, 5 h

2: 152 mg / 0.3 M aq. H₂SO₄ / acetone / 7 h / Heating

With n-butyllithium; sulfuric acid; In tetrahydrofuran; acetone;
DOI:10.1139/v81-311