Carbamic acid, (trimethylsilyl)-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, (trimethylsilyl)-, 1,1-dimethylethyl ester (9CI)
CAS No.:238096-95-2
Molecular Formula:C₈H₁₉NO₂Si
Molecular Weight:189.33
Hs Code.:
Mol file:238096-95-2.mol

Synonyms:Carbamicacid, (trimethylsilyl)-, 1,1-dimethylethyl ester (9CI)

Suppliers and Price of Carbamic acid, (trimethylsilyl)-, 1,1-dimethylethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
tert-butylN-(trimethylsilyl)carbamate
50mg
$ 65.00

Total 1 raw suppliers

Chemical Property of Carbamic acid, (trimethylsilyl)-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

PSA：38.33000
LogP:2.73690

Purity/Quality:: tert-butylN-(trimethylsilyl)carbamate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Carbamic acid, (trimethylsilyl)-, 1,1-dimethylethyl ester (9CI)

There total 1 articles about Carbamic acid, (trimethylsilyl)-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 75-77-4
chloro-trimethyl-silane

: 4248-19-5
tert-butyl carbazate

: 238096-95-2
N-trimethylsilyl O-tert-butyl carbamate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1246/cl.2011.326

Reference yield: 67.0%

: 80120-36-1
ethyl 2‐(4‐(tert‐butyl)phenyl)2‐oxoacetate

: 238096-95-2
N-trimethylsilyl O-tert-butyl carbamate

: ethyl (Z)-2-[(tert-butoxycarbonyl)imino]-2-[4-(tert-butyl)phenyl]acetate

Guidance literature:: N-trimethylsilyl O-tert-butyl carbamate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

ethyl 2‐(4‐(tert‐butyl)phenyl)2‐oxoacetate; In tetrahydrofuran; hexane; at -78 ℃; for 5h; Inert atmosphere;

With chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.202101114

Reference yield: 60.0%

: 40140-16-7
ethyl (p-methoxyphenyl)oxoacetate

: 238096-95-2
N-trimethylsilyl O-tert-butyl carbamate

: ethyl (Z)-2-[(tert-butoxycarbonyl)imino]-2-(4-methoxyphenyl)acetate

Guidance literature:: N-trimethylsilyl O-tert-butyl carbamate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

ethyl (p-methoxyphenyl)oxoacetate; In tetrahydrofuran; hexane; at -78 ℃; for 5h; Inert atmosphere;

With chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.202101114