benzyl 3,5-diazido-2-(benzyloxycarbonylamino)-2,3,5-trideoxy-β-D-ribofuranoside

Base Information

Chemical Name:benzyl 3,5-diazido-2-(benzyloxycarbonylamino)-2,3,5-trideoxy-β-D-ribofuranoside
CAS No.:74593-11-6
Molecular Formula:C₂₀H₂₁N₇O₄
Molecular Weight:423.431
Hs Code.:

Synonyms:benzyl 3,5-diazido-2-(benzyloxycarbonylamino)-2,3,5-trideoxy-β-D-ribofuranoside

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Chemical Property of benzyl 3,5-diazido-2-(benzyloxycarbonylamino)-2,3,5-trideoxy-β-D-ribofuranoside

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Technology Process of benzyl 3,5-diazido-2-(benzyloxycarbonylamino)-2,3,5-trideoxy-β-D-ribofuranoside

There total 2 articles about benzyl 3,5-diazido-2-(benzyloxycarbonylamino)-2,3,5-trideoxy-β-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 74593-10-5
benzyl 2-(benzyloxycarbonylamino)-2-deoxy-3,5-di-O-mesyl-β-D-xylofuranoside

: 74593-11-6
benzyl 3,5-diazido-2-(benzyloxycarbonylamino)-2,3,5-trideoxy-β-D-ribofuranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 80 - 85 ℃; for 12h;
DOI:10.1016/S0008-6215(00)85674-8

Reference yield:

: 66166-90-3
benzyl 2-(benzyloxycarbonylamino)-2-deoxy-β-D-xylofuranoside

: 74593-11-6
benzyl 3,5-diazido-2-(benzyloxycarbonylamino)-2,3,5-trideoxy-β-D-ribofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / pyridine / 3 h / 0 °C

2: 93 percent / sodium azide / dimethylformamide / 12 h / 80 - 85 °C

With pyridine; sodium azide; In N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)85674-8

Reference yield:

: 108-24-7
acetic anhydride

: 74593-11-6
benzyl 3,5-diazido-2-(benzyloxycarbonylamino)-2,3,5-trideoxy-β-D-ribofuranoside

: 74593-12-7
benzyl 2,3,5-triacetamido-2,3,5-trideoxy-β-D-ribofuranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; Yield given. Multistep reaction; 1.) methanol, 35 degC, 3 h; 2.) methanol, room temperature, 30 min;
DOI:10.1016/S0008-6215(00)85674-8