5-<4-<2-(6-Methyl-2-pyridyl)ethoxy>benzylidene>rhodanine-3-acetic Acid

Base Information

Chemical Name:5-<4-<2-(6-Methyl-2-pyridyl)ethoxy>benzylidene>rhodanine-3-acetic Acid
CAS No.:136401-73-5
Molecular Formula:C₂₀H₁₈N₂O₄S₂
Molecular Weight:414.506
Hs Code.:

Synonyms:5-<4-<2-(6-Methyl-2-pyridyl)ethoxy>benzylidene>rhodanine-3-acetic Acid

Suppliers and Price of 5-<4-<2-(6-Methyl-2-pyridyl)ethoxy>benzylidene>rhodanine-3-acetic Acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-<4-<2-(6-Methyl-2-pyridyl)ethoxy>benzylidene>rhodanine-3-acetic Acid

Chemical Property:

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Technology Process of 5-<4-<2-(6-Methyl-2-pyridyl)ethoxy>benzylidene>rhodanine-3-acetic Acid

There total 4 articles about 5-<4-<2-(6-Methyl-2-pyridyl)ethoxy>benzylidene>rhodanine-3-acetic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 5718-83-2
rhodanine 3-acetic acid

: 85259-44-5
4-<2-(6-methyl-2-pyridyl)ethoxy>benzaldehyde

: 136401-73-5
5-<4-<2-(6-Methyl-2-pyridyl)ethoxy>benzylidene>rhodanine-3-acetic Acid

Guidance literature:: With piperidine; In ethanol; for 1h; Heating;
DOI:10.1248/cpb.39.1440

Reference yield:

: 934-78-1
2-(6-methylpyridin-2-yl)-ethanol

: 136401-73-5
5-<4-<2-(6-Methyl-2-pyridyl)ethoxy>benzylidene>rhodanine-3-acetic Acid

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / NaH (oil susp.) / tetrahydrofuran / 2 h

2: 64 percent / Raney Ni, aq. HCOOH / 1 h / Heating

3: 75 percent / piperidine / ethanol / 1 h / Heating

With piperidine; formic acid; nickel; sodium hydride; In tetrahydrofuran; ethanol;
DOI:10.1248/cpb.39.1440

Reference yield:

: 1194-02-1,143234-87-1
4-fluorobenzonitrile

: 136401-73-5
5-<4-<2-(6-Methyl-2-pyridyl)ethoxy>benzylidene>rhodanine-3-acetic Acid

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / NaH (oil susp.) / tetrahydrofuran / 2 h

2: 64 percent / Raney Ni, aq. HCOOH / 1 h / Heating

3: 75 percent / piperidine / ethanol / 1 h / Heating

With piperidine; formic acid; nickel; sodium hydride; In tetrahydrofuran; ethanol;
DOI:10.1248/cpb.39.1440