4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid methyl-(4-methylsulfanyl-phenyl)-amide

Base Information

• Chemical Name: 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid methyl-(4-methylsulfanyl-phenyl)-amide
• CAS No.: 724733-01-1
• Molecular Formula: C₁₉H₁₄F₁₇NOS
• Molecular Weight: 627.365

Synonyms:4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid methyl-(4-methylsulfanyl-phenyl)-amide

Chemical Property of 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid methyl-(4-methylsulfanyl-phenyl)-amide

Chemical Property:

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Technology Process of 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid methyl-(4-methylsulfanyl-phenyl)-amide

There total 1 articles about 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid methyl-(4-methylsulfanyl-phenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

methyl iodide (74-88-4) + 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid [4-(4-amino-phenyldisulfanyl)-phenyl]-amide → 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid methyl-(4-methylsulfanyl-phenyl)-amide (724733-01-1)

Guidance literature:

With potassium hydroxide; tetrabutylammomium bromide; In tetrahydrofuran; water; at 20 ℃; for 15h;

DOI:10.1016/j.tetlet.2004.04.116

Reference yield: 100.0%

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid methyl-(4-methylsulfanyl-phenyl)-amide (724733-01-1) → 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid (4-methanesulfinyl-phenyl)-methyl-amide (724733-03-3)

Guidance literature:

With Selectfluor; In water; acetonitrile; at 20 ℃; for 0.333333h;

DOI:10.1016/j.tetlet.2004.04.116

upstream raw materials:

methyl iodide

Downstream raw materials:

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecanoic acid (4-methanesulfinyl-phenyl)-methyl-amide

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