N-((1R,2R)-2-(2-((4-methylcyclohexa-1,4-dienyl)methoxy)ethylamino)-1,2-diphenylethyl)-2-(trifluoromethyl)benzenesulfon amide hydrochloride

Base Information

Chemical Name:N-((1R,2R)-2-(2-((4-methylcyclohexa-1,4-dienyl)methoxy)ethylamino)-1,2-diphenylethyl)-2-(trifluoromethyl)benzenesulfon amide hydrochloride
CAS No.:1360897-64-8
Molecular Formula:C₃₁H₃₃F₃N₂O₃S*ClH
Molecular Weight:607.137
Hs Code.:

Synonyms:N-((1R,2R)-2-(2-((4-methylcyclohexa-1,4-dienyl)methoxy)ethylamino)-1,2-diphenylethyl)-2-(trifluoromethyl)benzenesulfon amide hydrochloride

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Chemical Property of N-((1R,2R)-2-(2-((4-methylcyclohexa-1,4-dienyl)methoxy)ethylamino)-1,2-diphenylethyl)-2-(trifluoromethyl)benzenesulfon amide hydrochloride

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Technology Process of N-((1R,2R)-2-(2-((4-methylcyclohexa-1,4-dienyl)methoxy)ethylamino)-1,2-diphenylethyl)-2-(trifluoromethyl)benzenesulfon amide hydrochloride

There total 4 articles about N-((1R,2R)-2-(2-((4-methylcyclohexa-1,4-dienyl)methoxy)ethylamino)-1,2-diphenylethyl)-2-(trifluoromethyl)benzenesulfon amide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.9%

: 1360897-62-6
N-((1R,2R)-2-(2-((4-methylcyclohexa-1,4-dienyl)methoxy)ethylamino)-1,2-diphenylethyl)-2-(trifluoromethyl)benzenesulfonamide

: 1360897-64-8
N-((1R,2R)-2-(2-((4-methylcyclohexa-1,4-dienyl)methoxy)ethylamino)-1,2-diphenylethyl)-2-(trifluoromethyl)benzenesulfon amide hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; dichloromethane; for 0.5h;

Reference yield:

: 78-79-5,9003-31-0
isoprene

: 1360897-64-8
N-((1R,2R)-2-(2-((4-methylcyclohexa-1,4-dienyl)methoxy)ethylamino)-1,2-diphenylethyl)-2-(trifluoromethyl)benzenesulfon amide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,2-bis-(diphenylphosphino)ethane; cobalt(II) bromide; zinc(II) iodide; zinc / tetrahydrofuran / 1 h / 35 °C

1.2: 1 h / 20 °C / Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / toluene / 14 h / 130 °C

2.2: 0.5 h

With N-ethyl-N,N-diisopropylamine; 1,2-bis-(diphenylphosphino)ethane; cobalt(II) bromide; zinc(II) iodide; zinc; In tetrahydrofuran; toluene;

Reference yield:

: 3973-18-0
2-(prop-2-ynyloxy)ethanol

: 1360897-64-8
N-((1R,2R)-2-(2-((4-methylcyclohexa-1,4-dienyl)methoxy)ethylamino)-1,2-diphenylethyl)-2-(trifluoromethyl)benzenesulfon amide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,2-bis-(diphenylphosphino)ethane; cobalt(II) bromide; zinc(II) iodide; zinc / tetrahydrofuran / 1 h / 35 °C

1.2: 1 h / 20 °C / Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / toluene / 14 h / 130 °C

2.2: 0.5 h

With N-ethyl-N,N-diisopropylamine; 1,2-bis-(diphenylphosphino)ethane; cobalt(II) bromide; zinc(II) iodide; zinc; In tetrahydrofuran; toluene;