butyl (S)-4-(2-benzyloxycarbonylamino-4-tert-butoxycarbonylbutyryl)piperazine-1-carboxylate

Base Information

Chemical Name:butyl (S)-4-(2-benzyloxycarbonylamino-4-tert-butoxycarbonylbutyryl)piperazine-1-carboxylate
CAS No.:1019929-05-5
Molecular Formula:C₂₆H₃₉N₃O₇
Molecular Weight:505.612
Hs Code.:

Synonyms:butyl (S)-4-(2-benzyloxycarbonylamino-4-tert-butoxycarbonylbutyryl)piperazine-1-carboxylate

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Chemical Property of butyl (S)-4-(2-benzyloxycarbonylamino-4-tert-butoxycarbonylbutyryl)piperazine-1-carboxylate

Chemical Property:

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Technology Process of butyl (S)-4-(2-benzyloxycarbonylamino-4-tert-butoxycarbonylbutyryl)piperazine-1-carboxylate

There total 6 articles about butyl (S)-4-(2-benzyloxycarbonylamino-4-tert-butoxycarbonylbutyryl)piperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 50606-32-1
1-butyloxycarbonylpiperazine

: 3886-08-6
5-tert-butyl N-benzyloxycarbonyl-L-glutamate

: 1019929-05-5
butyl (S)-4-(2-benzyloxycarbonylamino-4-tert-butoxycarbonylbutyryl)piperazine-1-carboxylate

Guidance literature:: 5-tert-butyl N-benzyloxycarbonyl-L-glutamate; With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 5 ℃;

1-butyloxycarbonylpiperazine; In dichloromethane; at 5 - 20 ℃;
DOI:10.1021/jm901518t

Reference yield:

: 1190713-19-9
Piperazine-1-carboxylic acid butyl ester hydrochloride salt

: 3886-08-6
5-tert-butyl N-benzyloxycarbonyl-L-glutamate

: 1019929-05-5
butyl (S)-4-(2-benzyloxycarbonylamino-4-tert-butoxycarbonylbutyryl)piperazine-1-carboxylate

Guidance literature:: 5-tert-butyl N-benzyloxycarbonyl-L-glutamate; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; at 20 ℃; for 0.0833333h;

Piperazine-1-carboxylic acid butyl ester hydrochloride salt; In tetrahydrofuran; dichloromethane; at 20 ℃;

Reference yield:

: 1073554-08-1
1-butoxy-carbonylpiperazine trifluoroacetate

: 3886-08-6
5-tert-butyl N-benzyloxycarbonyl-L-glutamate

: 1019929-05-5
butyl (S)-4-(2-benzyloxycarbonylamino-4-tert-butoxycarbonylbutyryl)piperazine-1-carboxylate

Guidance literature:: With N-ethylmorpholine;; O-<[cyano(ethoxycarbonyl)methylene]amino>-1,1,3,3-tetramethyluronium tetrafluoroborate; In N,N-dimethyl-formamide; for 12h;