17-(tert-butyldiphenylsiloxy)-1-hydroxy-3,6,9,12,15-pentaoxyheptadecane

Base Information

Chemical Name:17-(tert-butyldiphenylsiloxy)-1-hydroxy-3,6,9,12,15-pentaoxyheptadecane
CAS No.:176703-17-6
Molecular Formula:C₂₈H₄₄O₇Si
Molecular Weight:520.739
Hs Code.:

Synonyms:17-(tert-butyldiphenylsiloxy)-1-hydroxy-3,6,9,12,15-pentaoxyheptadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 17-(tert-butyldiphenylsiloxy)-1-hydroxy-3,6,9,12,15-pentaoxyheptadecane

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Technology Process of 17-(tert-butyldiphenylsiloxy)-1-hydroxy-3,6,9,12,15-pentaoxyheptadecane

There total 1 articles about 17-(tert-butyldiphenylsiloxy)-1-hydroxy-3,6,9,12,15-pentaoxyheptadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 2615-15-8
pentaethylene glycol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 176703-17-6
17-(tert-butyldiphenylsiloxy)-1-hydroxy-3,6,9,12,15-pentaoxyheptadecane

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; for 3h;
DOI:10.1016/j.tet.2005.08.085

Reference yield: 87.0%

: 2,2-dimethylpent-4-enyl chloroformate

: 176703-17-6
17-(tert-butyldiphenylsiloxy)-1-hydroxy-3,6,9,12,15-pentaoxyheptadecane

: 678143-02-7
1-(tert-butyldiphenylsiloxy)-22,22-dimethyl-19-oxo-3,6,9,12,15,17,19-heptaoxapentacos-24-ene

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;

Reference yield: 35.0%

: 115208-40-7
(5α,20S)-3-oxopregnane-20-carboxylic acid

: 176703-17-6
17-(tert-butyldiphenylsiloxy)-1-hydroxy-3,6,9,12,15-pentaoxyheptadecane

: 869893-55-0
(S)-2-((5S,8R,9S,10S,13S,14S,17R)-10,13-Dimethyl-3-oxo-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-propionic acid 2-{2-[2-(2-{2-[2-(tert-butyl-diphenyl-silanyloxy)-ethoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-ethyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 16h;
DOI:10.1016/j.tet.2005.08.085