2-(4-methoxyphenyl)-8-methyl-1-tosyl-1,2,3,8-tetrahydropyrrolo[2,3-b]indole

Base Information

Chemical Name:2-(4-methoxyphenyl)-8-methyl-1-tosyl-1,2,3,8-tetrahydropyrrolo[2,3-b]indole
CAS No.:1562571-01-0
Molecular Formula:C₂₅H₂₄N₂O₃S
Molecular Weight:432.543
Hs Code.:

Synonyms:2-(4-methoxyphenyl)-8-methyl-1-tosyl-1,2,3,8-tetrahydropyrrolo[2,3-b]indole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-methoxyphenyl)-8-methyl-1-tosyl-1,2,3,8-tetrahydropyrrolo[2,3-b]indole

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Technology Process of 2-(4-methoxyphenyl)-8-methyl-1-tosyl-1,2,3,8-tetrahydropyrrolo[2,3-b]indole

There total 3 articles about 2-(4-methoxyphenyl)-8-methyl-1-tosyl-1,2,3,8-tetrahydropyrrolo[2,3-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 637-69-4,24936-44-5
4-Methoxystyrene

: 1562569-28-1
4-methyl-3-tosyl-3,4-dihydro-[1,2,3]triazolo[4,5-b]indole

: 1562571-01-0
2-(4-methoxyphenyl)-8-methyl-1-tosyl-1,2,3,8-tetrahydropyrrolo[2,3-b]indole

Guidance literature:: With rhodium (II) octanoate dimer; In 1,2-dichloro-ethane; for 6h; regioselective reaction; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1021/ol5002347

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1562571-01-0
2-(4-methoxyphenyl)-8-methyl-1-tosyl-1,2,3,8-tetrahydropyrrolo[2,3-b]indole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / ethanol; water / 3 h / 20 °C / Heating

2: copper(l) chloride; triethylamine / acetonitrile / 3 h / 20 °C / Inert atmosphere; Schlenk technique

3: rhodium (II) octanoate dimer / 1,2-dichloro-ethane / 6 h / Inert atmosphere; Schlenk technique; Reflux

With sodium azide; rhodium (II) octanoate dimer; triethylamine; copper(l) chloride; In ethanol; water; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/ol5002347

Reference yield:

: 941-55-9
4-toluenesulfonyl azide

: 1562571-01-0
2-(4-methoxyphenyl)-8-methyl-1-tosyl-1,2,3,8-tetrahydropyrrolo[2,3-b]indole

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) chloride; triethylamine / acetonitrile / 3 h / 20 °C / Inert atmosphere; Schlenk technique

2: rhodium (II) octanoate dimer / 1,2-dichloro-ethane / 6 h / Inert atmosphere; Schlenk technique; Reflux

With rhodium (II) octanoate dimer; triethylamine; copper(l) chloride; In 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/ol5002347