N,N'-bis(ethyl-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

Base Information

Chemical Name:N,N'-bis(ethyl-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide
CAS No.:1150097-60-1
Molecular Formula:C₄₉H₅₄N₂O₁₂S₂
Molecular Weight:927.106
Hs Code.:

Synonyms:N,N'-bis(ethyl-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

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Chemical Property of N,N'-bis(ethyl-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

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Technology Process of N,N'-bis(ethyl-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

There total 1 articles about N,N'-bis(ethyl-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1062080-87-8
N,N'-bis(ethyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

: 98-88-4
benzoyl chloride

: 1150097-60-1
N,N'-bis(ethyl-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

Guidance literature:: With pyridine; for 2h;
DOI:10.1002/ejoc.200801035

Reference yield: 84.0%

: 1150097-60-1
N,N'-bis(ethyl-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide

: 1150097-62-3
C₄₅H₄₂N₂O₁₂

Guidance literature:: N,N'-bis(ethyl-3-O-benzoyl-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranosid-2-yl)dimethylmalonamide; In dichloromethane; for 1h; Molecular sieve; Inert atmosphere;

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -30 ℃; for 1h; Inert atmosphere; Molecular sieve;
DOI:10.1002/ejoc.200801035