7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

Base Information

Chemical Name:7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride
CAS No.:1373491-58-7
Molecular Formula:C₂₂H₂₈ClNO₃*ClH
Molecular Weight:426.383
Hs Code.:

Synonyms:7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

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Chemical Property of 7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

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Technology Process of 7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

There total 11 articles about 7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.8%

: 1373491-76-9
7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester

: 1373491-58-7
7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

Guidance literature:: 7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester; With water; sodium hydroxide; In ethanol; for 6.5h; Reflux;

With hydrogenchloride; In water; pH=6;

Reference yield:

: 1121-46-6
2-Furan-2-yl-ethylamine

: 1373491-58-7
7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1.1: water / 0.5 h / 20 °C

2.1: hydrogenchloride / N,N-dimethyl-formamide / Saturated solution

2.2: pH 11

3.1: dichloromethane / 1.5 h / 20 °C

4.1: hydrogenchloride / methanol / 5.5 h / 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 65 °C / Inert atmosphere

6.1: sodium hydroxide; water / ethanol / 6.5 h / Reflux

6.2: pH 6

With hydrogenchloride; water; potassium carbonate; sodium hydroxide; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 98-01-1
furfural

: 1373491-58-7
7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid hydrochloride

Guidance literature:: Multi-step reaction with 8 steps

1.1: ammonium acetate / 0.75 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere; Reflux

3.1: water / 0.5 h / 20 °C

4.1: hydrogenchloride / N,N-dimethyl-formamide / Saturated solution

4.2: pH 11

5.1: dichloromethane / 1.5 h / 20 °C

6.1: hydrogenchloride / methanol / 5.5 h / 20 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 65 °C / Inert atmosphere

8.1: sodium hydroxide; water / ethanol / 6.5 h / Reflux

8.2: pH 6

With hydrogenchloride; lithium aluminium tetrahydride; ammonium acetate; water; potassium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;