7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester

Base Information

Chemical Name:7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester
CAS No.:1373491-76-9
Molecular Formula:C₂₄H₃₂ClNO₃
Molecular Weight:417.976
Hs Code.:

Synonyms:7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester

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Chemical Property of 7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester

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Technology Process of 7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester

There total 10 articles about 7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.1%

: 4,5,6,7-tetrahydrofuro[3,2-c]pyridine hydrochloride

: 1373492-27-3
7-bromo-7-(2-chlorophenyl)-2,2-dimethylheptanoic acid ethyl ester

: 1373491-76-9
7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 65 ℃; Inert atmosphere;

Reference yield:

: 1121-46-6
2-Furan-2-yl-ethylamine

: 1373491-76-9
7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: water / 0.5 h / 20 °C

2.1: hydrogenchloride / N,N-dimethyl-formamide / Saturated solution

2.2: pH 11

3.1: dichloromethane / 1.5 h / 20 °C

4.1: hydrogenchloride / methanol / 5.5 h / 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 65 °C / Inert atmosphere

With hydrogenchloride; potassium carbonate; In methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 98-01-1
furfural

: 1373491-76-9
7-(2-chlorophenyl)-7-(6,7-dihydro-4H-furo[3,2-c]pyridin-5-yl)-2,2-dimethylheptanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1.1: ammonium acetate / 0.75 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere; Reflux

3.1: water / 0.5 h / 20 °C

4.1: hydrogenchloride / N,N-dimethyl-formamide / Saturated solution

4.2: pH 11

5.1: dichloromethane / 1.5 h / 20 °C

6.1: hydrogenchloride / methanol / 5.5 h / 20 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 65 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; ammonium acetate; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;