6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratraldehyde

Base Information

Chemical Name:6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratraldehyde
CAS No.:142609-33-4
Molecular Formula:C₂₁H₂₂F₃NO₆
Molecular Weight:441.404
Hs Code.:

Synonyms:6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratraldehyde

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Chemical Property of 6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratraldehyde

Chemical Property:

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Technology Process of 6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratraldehyde

There total 5 articles about 6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratraldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 5392-10-9
2-bromo-4,5-dimethoxybenzaldehyde

: 142609-32-3
N-methyl-N-trifluoroacetyl-3-hydroxy-4-methoxyphenethylamine

: 142609-33-4
6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratraldehyde

Guidance literature:: With pyridine; potassium carbonate; copper(II) oxide; for 13h; Heating;

Reference yield:

: 68360-20-3
N-formyl-3-benzyloxy-4-methoxyphenethylamine

: 142609-33-4
6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratraldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 382 mg / LiAlH₄ / tetrahydrofuran; diethyl ether / 1.) 20 min, RT, 2.) 50 deg C, 6 h

2: K₂CO₃ / CH₂Cl₂ / 1 h / Ambient temperature

3: 85 percent / H₂ / 2percent PdCl₂, C / methanol / 760 Torr

4: 49 percent / K₂CO₃, CuO, pyridine / 13 h / Heating

With pyridine; lithium aluminium tetrahydride; hydrogen; potassium carbonate; copper(II) oxide; palladium dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;

Reference yield:

: 36455-21-7
3-benzyloxy-4-methoxyphenylethylamine

: 142609-33-4
6-<5-β-(N-methyl-N-trifluoroacetylamino)ethyl-2-methoxy>phenyloxyveratraldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / 6 h / Heating

2: 382 mg / LiAlH₄ / tetrahydrofuran; diethyl ether / 1.) 20 min, RT, 2.) 50 deg C, 6 h

3: K₂CO₃ / CH₂Cl₂ / 1 h / Ambient temperature

4: 85 percent / H₂ / 2percent PdCl₂, C / methanol / 760 Torr

5: 49 percent / K₂CO₃, CuO, pyridine / 13 h / Heating

With pyridine; lithium aluminium tetrahydride; hydrogen; potassium carbonate; copper(II) oxide; palladium dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;