7-methyl 1-deoxy-1-{[(2,4-dichlorophenoxy)acethyl]amino}-2,3,4-tri-O-acetyl-β-D-glucopyranuronate

Base Information

Chemical Name:7-methyl 1-deoxy-1-{[(2,4-dichlorophenoxy)acethyl]amino}-2,3,4-tri-O-acetyl-β-D-glucopyranuronate
CAS No.:500339-96-8
Molecular Formula:C₂₁H₂₃Cl₂NO₁₁
Molecular Weight:536.32
Hs Code.:

Synonyms:7-methyl 1-deoxy-1-{[(2,4-dichlorophenoxy)acethyl]amino}-2,3,4-tri-O-acetyl-β-D-glucopyranuronate

Suppliers and Price of 7-methyl 1-deoxy-1-{[(2,4-dichlorophenoxy)acethyl]amino}-2,3,4-tri-O-acetyl-β-D-glucopyranuronate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-methyl 1-deoxy-1-{[(2,4-dichlorophenoxy)acethyl]amino}-2,3,4-tri-O-acetyl-β-D-glucopyranuronate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-methyl 1-deoxy-1-{[(2,4-dichlorophenoxy)acethyl]amino}-2,3,4-tri-O-acetyl-β-D-glucopyranuronate

There total 2 articles about 7-methyl 1-deoxy-1-{[(2,4-dichlorophenoxy)acethyl]amino}-2,3,4-tri-O-acetyl-β-D-glucopyranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 94-75-7,89300-30-1
2,4-Dichlorophenoxyacetic acid

: 14365-73-2
2,3,4-tri-O-acetyl-β-D-glucopyranosylamine uronic acid methyl ester

: 500339-96-8
7-methyl 1-deoxy-1-{[(2,4-dichlorophenoxy)acethyl]amino}-2,3,4-tri-O-acetyl-β-D-glucopyranuronate

Guidance literature:: With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1016/j.carres.2004.05.024

Reference yield:

: 67776-38-9,163776-36-1
2,3,4-tri-O-acetyl-1-azido-1-deoxy-β-D-glucopyranuronic acid methyl ester

: 500339-96-8
7-methyl 1-deoxy-1-{[(2,4-dichlorophenoxy)acethyl]amino}-2,3,4-tri-O-acetyl-β-D-glucopyranuronate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / tetrahydrofuran / -5 °C

2: 12 percent / HOBT; DMAP; DCC / tetrahydrofuran / 12 h / 20 °C

With dmap; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1016/j.carres.2004.05.024