{3-[methoxy(tricyclo[3.3.1.13,7]dec-2-ylidene)methyl]phenoxy}(dimethyl)(2-methyl-2-propanyl)silane

Base Information

Chemical Name:{3-[methoxy(tricyclo[3.3.1.13,7]dec-2-ylidene)methyl]phenoxy}(dimethyl)(2-methyl-2-propanyl)silane
CAS No.:111807-81-9
Molecular Formula:C₂₄H₃₆O₂Si
Molecular Weight:384.634
Hs Code.:

Synonyms:{3-[methoxy(tricyclo[3.3.1.13,7]dec-2-ylidene)methyl]phenoxy}(dimethyl)(2-methyl-2-propanyl)silane

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Chemical Property of {3-[methoxy(tricyclo[3.3.1.13,7]dec-2-ylidene)methyl]phenoxy}(dimethyl)(2-methyl-2-propanyl)silane

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Technology Process of {3-[methoxy(tricyclo[3.3.1.13,7]dec-2-ylidene)methyl]phenoxy}(dimethyl)(2-methyl-2-propanyl)silane

There total 14 articles about {3-[methoxy(tricyclo[3.3.1.13,7]dec-2-ylidene)methyl]phenoxy}(dimethyl)(2-methyl-2-propanyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 700-58-3
2-Adamantanone

: dimethyl((3-((tertbutyldimethylsilyl)oxy)phenyl)(methoxy)methyl)phosphonate

: 111807-81-9
{3-[methoxy(tricyclo[3.3.1.13,7]dec-2-ylidene)methyl]phenoxy}(dimethyl)(2-methyl-2-propanyl)silane

Guidance literature:: dimethyl((3-((tertbutyldimethylsilyl)oxy)phenyl)(methoxy)methyl)phosphonate; With lithium diisopropyl amide; In tetrahydrofuran; at -65 ℃; for 0.333333h; Inert atmosphere;

2-Adamantanone; In tetrahydrofuran; at -65 ℃; for 0.25h;
DOI:10.1039/c9ob01407a

Reference yield: 83.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 121445-45-2
[(3-hydroxyphenyl)methoxymethylene]tricyclo[3.3.1.13.7]-decane

: 111807-81-9
{3-[methoxy(tricyclo[3.3.1.13,7]dec-2-ylidene)methyl]phenoxy}(dimethyl)(2-methyl-2-propanyl)silane

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃; for 17h;
DOI:10.1016/j.tet.2017.05.084

Reference yield: 59.0%

: 700-58-3
2-Adamantanone

: 120687-94-7
3-t-butyldimethylsilyloxybenzoic acid methyl ester

: 111807-81-9
{3-[methoxy(tricyclo[3.3.1.13,7]dec-2-ylidene)methyl]phenoxy}(dimethyl)(2-methyl-2-propanyl)silane

Guidance literature:: With lithium aluminium tetrahydride; titanium(III) chloride; triethylamine; In tetrahydrofuran; at 70 ℃; for 20h;
DOI:10.1016/S0040-4039(02)00617-2