C₃₃H₃₁ClFN₃O₉S

Base Information

Chemical Name:C₃₃H₃₁ClFN₃O₉S
CAS No.:1417792-20-1
Molecular Formula:C₃₃H₃₁ClFN₃O₉S
Molecular Weight:700.141
Hs Code.:

C<sub>33</sub>H<sub>31</sub>ClFN<sub>3</sub>O<sub>9</sub>S

Synonyms:C₃₃H₃₁ClFN₃O₉S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₃₁ClFN₃O₉S

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Technology Process of C₃₃H₃₁ClFN₃O₉S

There total 10 articles about C₃₃H₃₁ClFN₃O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 1417792-37-0
C₃₅H₃₅ClFN₃O₉S

: 1417792-20-1
C₃₃H₃₁ClFN₃O₉S

Guidance literature:: With water; potassium carbonate; In methanol; at 80 ℃; for 0.0833333h;
DOI:10.1021/jm3014844

Reference yield:

: 73781-91-6
6-Chloronicotinic acid methyl ester

: 1417792-20-1
C₃₃H₃₁ClFN₃O₉S

Guidance literature:: Multi-step reaction with 6 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,4-dioxane / 80 °C / Inert atmosphere

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.33 h / 20 - 60 °C

3: palladium on activated charcoal; hydrogen / methanol / 0.25 h / 20 °C

4: triethylamine / tetrahydrofuran / -20 °C

5: tetrahydrofuran / 0.08 h / 100 °C

6: potassium carbonate; water / methanol / 0.08 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; di-isopropyl azodicarboxylate; palladium on activated charcoal; water; hydrogen; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; 1: |Suzuki Coupling / 2: |Mitsunobu Displacement;
DOI:10.1021/jm3014844

Reference yield:

: 1089280-66-9
1-chloro-2-fluoro-4-methoxy-5-nitrobenzene

: 1417792-20-1
C₃₃H₃₁ClFN₃O₉S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 °C

1.2: 0.25 h / 60 °C

2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.33 h / 20 - 60 °C

3.1: palladium on activated charcoal; hydrogen / methanol / 0.25 h / 20 °C

4.1: triethylamine / tetrahydrofuran / -20 °C

5.1: tetrahydrofuran / 0.08 h / 100 °C

6.1: potassium carbonate; water / methanol / 0.08 h / 80 °C

With di-isopropyl azodicarboxylate; palladium on activated charcoal; water; hydrogen; sodium hydride; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; mineral oil; 2.1: |Mitsunobu Displacement;
DOI:10.1021/jm3014844