methyl (R)-2-((R)-2-(benzyloxycarbonylamino)-3-phenylpropanamido)-4-methylvalerate

Base Information

Chemical Name:methyl (R)-2-((R)-2-(benzyloxycarbonylamino)-3-phenylpropanamido)-4-methylvalerate
CAS No.:37894-30-7
Molecular Formula:C₂₄H₃₀N₂O₅
Molecular Weight:426.513
Hs Code.:

Synonyms:methyl (R)-2-((R)-2-(benzyloxycarbonylamino)-3-phenylpropanamido)-4-methylvalerate

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Chemical Property of methyl (R)-2-((R)-2-(benzyloxycarbonylamino)-3-phenylpropanamido)-4-methylvalerate

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Technology Process of methyl (R)-2-((R)-2-(benzyloxycarbonylamino)-3-phenylpropanamido)-4-methylvalerate

There total 5 articles about methyl (R)-2-((R)-2-(benzyloxycarbonylamino)-3-phenylpropanamido)-4-methylvalerate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2448-45-5
Cbz-D-Phe

: 5845-53-4,6322-53-8,7517-19-3
(R)-leucine methyl ester hydrochloride

: 37894-30-7
methyl (R)-2-((R)-2-(benzyloxycarbonylamino)-3-phenylpropanamido)-4-methylvalerate

Guidance literature:: With copper(II) choride dihydrate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at -5 - 0 ℃; Inert atmosphere;

Reference yield:

: 23032-21-5
D-leucine methyl ester

: 37894-30-7
methyl (R)-2-((R)-2-(benzyloxycarbonylamino)-3-phenylpropanamido)-4-methylvalerate

Guidance literature:: With diethyl ether;
DOI:10.1021/ja01855a020

Reference yield:

: 328-38-1,21675-61-6,25248-98-0,70-45-1
(R)-leucine

: 37894-30-7
methyl (R)-2-((R)-2-(benzyloxycarbonylamino)-3-phenylpropanamido)-4-methylvalerate

Guidance literature:: Multi-step reaction with 2 steps

1: HCl

2: diethyl ether

With hydrogenchloride; diethyl ether;
DOI:10.1021/ja01855a020