2-ETHYL-2-METHYLACETOACETIC ACID ETHYL ESTER

Base Information

• Chemical Name: 2-ETHYL-2-METHYLACETOACETIC ACID ETHYL ESTER
• CAS No.: 33697-53-9
• Molecular Formula: C9H16 O3
• Molecular Weight: 172.224
• Hs Code.: 2918300090
• Mol file: 33697-53-9.mol

Synonyms:Acetoaceticacid, 2-ethyl-2-methyl-, ethyl ester (6CI,8CI); Ethyl2-methyl-2-ethylacetoacetate

Chemical Property of 2-ETHYL-2-METHYLACETOACETIC ACID ETHYL ESTER

Chemical Property:

• Vapor Pressure: 0.352mmHg at 25°C
• Refractive Index: 1.425
• Boiling Point: 199 °C
• Flash Point: 74.1°C
• PSA: 43.37000
• Density: 0,98 g/cm3
• LogP: 1.55480

Purity/Quality:

98% ^*data from raw suppliers

Ethyl2-Ethyl-2-methyl-3-oxobutyrate ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-ETHYL-2-METHYLACETOACETIC ACID ETHYL ESTER

There total 4 articles about 2-ETHYL-2-METHYLACETOACETIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-acetylpropanoic acid ethyl ester (609-14-3) → ethyl 2-ethyl-2-methylacetoacetate (33697-53-9)

Guidance literature:

With sodium hydride;

Reference yield:

→ ethyl 2-ethyl-2-methylacetoacetate (33697-53-9)

Guidance literature:

With sodium hydride; N,N-dimethyl-formamide; benzene; anschliessend mit Methyljodid;

DOI:10.1021/jo01108a605

Reference yield:

methyl iodide (74-88-4) → ethyl 2-ethyl-2-methylacetoacetate (33697-53-9)

Guidance literature:

With benzene;

upstream raw materials:

methyl iodide

ethyl iodide

2-acetylpropanoic acid ethyl ester

Downstream raw materials:

Ethyl isovalerate

ethyl acetate

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