3(S)-amino>-2-oxopiperidine

Base Information

Chemical Name:3(S)-amino>-2-oxopiperidine
CAS No.:114200-46-3
Molecular Formula:C₂₄H₃₄N₄O₅
Molecular Weight:458.558
Hs Code.:

3(S)-<N-<(benzyloxycarbonyl)-L-prolyl-L-leucyl>amino>-2-oxopiperidine

Synonyms:3(S)-amino>-2-oxopiperidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3(S)-amino>-2-oxopiperidine

Chemical Property:

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Technology Process of 3(S)-amino>-2-oxopiperidine

There total 4 articles about 3(S)-amino>-2-oxopiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1634-90-8
(S)-2-((S)-1-((benzyloxy)carbonyl)pyrrolidine-2-carboxamido)-4-methylpentanoic acid

: 42538-31-8,406216-02-2
(3S)-3-aminopiperidin-2-one hydrochloride

: 114200-46-3
3(S)-amino>-2-oxopiperidine

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In N,N-dimethyl-formamide; 1) 0 deg C, 2 d; 2) room temperature, 12 h;
DOI:10.1021/jm00402a031

Reference yield:

: 2480-95-7
methyl (S)-5-(((benzyloxy)carbonyl)amino)-2-((tertbutoxycarbonyl)amino)pentanoate

: 114200-46-3
3(S)-amino>-2-oxopiperidine

Guidance literature:: Multi-step reaction with 4 steps

1: AcOH, H₂ / Pd/C / methanol / 1 h / 2068.6 Torr

2: Na₂CO₃ / dimethylformamide / 48 h

3: 99 percent / HCl / ethyl acetate / 1 h / 0 °C

4: 55 percent / diphenyl phosphorazidate, Et₃N / dimethylformamide / 1) 0 deg C, 2 d; 2) room temperature, 12 h

With hydrogenchloride; diphenyl phosphoryl azide; hydrogen; sodium carbonate; acetic acid; triethylamine; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00402a031

Reference yield:

: 78397-39-4
Boc-Orn-OMe

: 114200-46-3
3(S)-amino>-2-oxopiperidine

Guidance literature:: Multi-step reaction with 3 steps

1: Na₂CO₃ / dimethylformamide / 48 h

2: 99 percent / HCl / ethyl acetate / 1 h / 0 °C

3: 55 percent / diphenyl phosphorazidate, Et₃N / dimethylformamide / 1) 0 deg C, 2 d; 2) room temperature, 12 h

With hydrogenchloride; diphenyl phosphoryl azide; sodium carbonate; triethylamine; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00402a031