cyclohexylmercapto-acetyl chloride

Base Information

• Chemical Name: cyclohexylmercapto-acetyl chloride
• CAS No.: 857570-47-9
• Molecular Formula: C₈H₁₃ClOS
• Molecular Weight: 192.71
• Mol file: 857570-47-9.mol

Synonyms:cyclohexylmercapto-acetyl chloride

Chemical Property of cyclohexylmercapto-acetyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of cyclohexylmercapto-acetyl chloride

There total 1 articles about cyclohexylmercapto-acetyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-cyclohexylthioacetic acid (52363-15-2) → cyclohexylmercapto-acetyl chloride (857570-47-9)

Guidance literature:

With thionyl chloride; triethylamine; In chloroform; for 2h; Heating;

DOI:10.1002/anie.200704349

Reference yield: 95.0%

cyclohexylmercapto-acetyl chloride (857570-47-9) + (S)-4-isopropylthiazolidine-2-thione (76186-04-4) → 3-((cyclohexylthio)acetyl)-4(S)-isopropyl-1,3-thiazolidine-2-thione (132288-44-9)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature;

DOI:10.1016/S0040-4020(01)96008-9

Reference yield:

Thiomorpholin (123-90-0) + cyclohexylmercapto-acetyl chloride (857570-47-9) → 2-(cyclohexylthio)-1-thiomorpholinoethanone (1015005-27-2)

Guidance literature:

With triethylamine; In chloroform; for 2h;

DOI:10.1002/anie.200704349

upstream raw materials:

2-cyclohexylthioacetic acid

Downstream raw materials:

3-((cyclohexylthio)acetyl)-4(S)-isopropyl-1,3-thiazolidine-2-thione

3-(2-(1-methyl-5-oxo-2-pyrrolidinyl)(cyclohexylthio)acetyl)-4(S)-isopropyl-1,3-thiazolidine-2-thione

2-(cyclohexylthio)-1-thiomorpholinoethanone