Technology Process of C35H36O8
There total 13 articles about C35H36O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridinium p-toluenesulfonate;
In
1,2-dichloro-ethane;
at 65 ℃;
for 1h;
Inert atmosphere;
DOI:10.1016/j.tetasy.2013.02.012
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 0 °C
2: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 2 h / 65 °C
With
tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; acetic acid;
In
tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1016/j.tetlet.2012.01.054
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C
1.2: 1.08 h / 0 - 20 °C
1.3: 0 °C
2.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / tetrahydrofuran; ethanol / 5.08 h / -40 - 0 °C
3.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / 20 °C
4.1: AD-mix-α; methanesulfonamide; water / tetrahydrofuran; tert-butyl alcohol / 16 h / 0 - 20 °C
5.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 0 °C
6.1: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 2 h / 65 °C
With
1H-imidazole; sodium tetrahydroborate; methanesulfonamide; cerium(III) chloride heptahydrate; AD-mix-α; tetrabutyl ammonium fluoride; water; pyridinium p-toluenesulfonate; sodium hydride; acetic acid;
In
tetrahydrofuran; ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol;
4.1: Sharpless dihydroxylation;
DOI:10.1016/j.tetlet.2012.01.054
