Technology Process of Nonanamide, N-(2-aminoethyl)-9-(.alpha.-D-mannopyranosyloxy)-
There total 6 articles about Nonanamide, N-(2-aminoethyl)-9-(.alpha.-D-mannopyranosyloxy)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 21 percent / 4A molecular sieves; calcium hypochlorite; acetic acid / acetonitrile / 20 °C
2: 86 percent / 4A molecular sieves; Me3SiOTf / CH2Cl2 / 2 h / 20 °C
3: 85 percent / K2CO3 / methanol
4: 95 percent / 36 h / 60 °C
With
calcium hypochlorite; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; potassium carbonate; acetic acid;
In
methanol; dichloromethane; acetonitrile;
1: Oxidation / 2: Substitution / 3: deprotection / 4: Acylation;
DOI:10.1016/S0008-6215(98)00330-9
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 86 percent / 4A molecular sieves; Me3SiOTf / CH2Cl2 / 2 h / 20 °C
2: 85 percent / K2CO3 / methanol
3: 95 percent / 36 h / 60 °C
With
trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; potassium carbonate;
In
methanol; dichloromethane;
1: Substitution / 2: deprotection / 3: Acylation;
DOI:10.1016/S0008-6215(98)00330-9
