octanedioic acid monobenzyl ester

Base Information

• Chemical Name: octanedioic acid monobenzyl ester
• CAS No.: 15570-39-5
• Molecular Formula: C₁₅H₂₀O₄
• Molecular Weight: 264.321

Synonyms:octanedioic acid monobenzyl ester

Chemical Property of octanedioic acid monobenzyl ester

Chemical Property:

Purity/Quality:

99%, ^*data from raw suppliers

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Technology Process of octanedioic acid monobenzyl ester

There total 6 articles about octanedioic acid monobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

octane-1,8-dioic acid (505-48-6) + benzyl alcohol (100-51-6,185532-71-2) → octanedioic acid monobenzyl ester (15570-39-5)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.bmcl.2021.127884

Reference yield: 65.0%

octane-1,8-dioic acid (505-48-6) + benzyl bromide (100-39-0) → octanedioic acid monobenzyl ester (15570-39-5)

Guidance literature:

With tetrabutylammomium bromide; potassium hydroxide; In methanol; Inert atmosphere;

DOI:10.1055/s-0034-1378345

Reference yield:

octane-1,8-dioic acid (505-48-6) + benzyl alcohol (100-51-6,185532-71-2) → octanedioic acid dibenzyl ester (42413-23-0) + dibenzyl ether (103-50-4) + octanedioic acid monobenzyl ester (15570-39-5)

Guidance literature:

Microwave irradiation;

DOI:10.1134/S1070363208100162

upstream raw materials:

octane-1,8-dioic acid

benzyl alcohol

benzyl bromide

3,3'-dithiobis(propionic acid)

Downstream raw materials:

Korksaeure-benzylester-(2-diethylamino-ethylester)

benzyl 8-[2-(tert-butoxycarbonylamino)ethylamino]-8-oxooctanoate

benzyl 8-(3-methoxy-3-oxopropylamino)-8-oxooctanoate

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