(R)-4-methylbenzenesulfinic acid[2-(4-chlorophenyl)-2-methylpropylidene]-amide

Base Information

Chemical Name:(R)-4-methylbenzenesulfinic acid[2-(4-chlorophenyl)-2-methylpropylidene]-amide
CAS No.:853680-36-1
Molecular Formula:C₁₇H₁₈ClNOS
Molecular Weight:319.855
Hs Code.:

Synonyms:(R)-4-methylbenzenesulfinic acid[2-(4-chlorophenyl)-2-methylpropylidene]-amide

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Chemical Property of (R)-4-methylbenzenesulfinic acid[2-(4-chlorophenyl)-2-methylpropylidene]-amide

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Technology Process of (R)-4-methylbenzenesulfinic acid[2-(4-chlorophenyl)-2-methylpropylidene]-amide

There total 2 articles about (R)-4-methylbenzenesulfinic acid[2-(4-chlorophenyl)-2-methylpropylidene]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6258-30-6
2-(4-chlorophenyl)-2-methylpropanoic acid

: 853680-36-1
(R)-4-methylbenzenesulfinic acid[2-(4-chlorophenyl)-2-methylpropylidene]-amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran / 3 h / 20 °C / Heating / reflux

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2 h / -78 °C

2.2: 3 h / 20 °C

3.1: titanium(IV) tetraethanolate / dichloromethane / 4 h / Heating / reflux

With titanium(IV) tetraethanolate; oxalyl dichloride; dimethyl sulfoxide; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; dichloromethane;

Reference yield:

: 80854-14-4
2-(4-chlorophenyl)-2-methylpropyl alcohol

: 853680-36-1
(R)-4-methylbenzenesulfinic acid[2-(4-chlorophenyl)-2-methylpropylidene]-amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2 h / -78 °C

1.2: 3 h / 20 °C

2.1: titanium(IV) tetraethanolate / dichloromethane / 4 h / Heating / reflux

With titanium(IV) tetraethanolate; oxalyl dichloride; dimethyl sulfoxide; In dichloromethane;