(2E)-3-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)-2-propenenitrile

Base Information

Chemical Name:(2E)-3-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)-2-propenenitrile
CAS No.:1380429-29-7
Molecular Formula:C₁₆H₉ClF₃NO
Molecular Weight:323.702
Hs Code.:

Synonyms:(2E)-3-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)-2-propenenitrile

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Chemical Property of (2E)-3-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)-2-propenenitrile

Chemical Property:

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Technology Process of (2E)-3-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)-2-propenenitrile

There total 3 articles about (2E)-3-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)-2-propenenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 516481-95-1
4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}benzaldehyde

: 16640-68-9
cyanomethylene triphenylphosphorane

: 1380429-29-7
(2E)-3-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)-2-propenenitrile

Guidance literature:: With sodium hydroxide; In dichloromethane; water; at 0 - 20 ℃; for 4h;

Reference yield:

: 6294-93-5
4-chloro-3-trifluoromethylphenol

: 1380429-29-7
(2E)-3-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)-2-propenenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0.33 h / 120 °C / Microwave irradiation

2: sodium hydroxide / dichloromethane; water / 4 h / 0 - 20 °C

With potassium carbonate; sodium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide; 2: Wittig Reaction;

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 1380429-29-7
(2E)-3-(4-{[4-chloro-3-(trifluoromethyl)phenyl]oxy}phenyl)-2-propenenitrile

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0.33 h / 120 °C / Microwave irradiation

2: sodium hydroxide / dichloromethane; water / 4 h / 0 - 20 °C

With potassium carbonate; sodium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide; 2: Wittig Reaction;