(2S,3R,4R)-2-Benzyloxy-5-(tert-butyldiphenylsiloxy)-4-dibenzylamino-3-hydroxy-N-methoxy-N-methylpentanamide

Base Information

Chemical Name:(2S,3R,4R)-2-Benzyloxy-5-(tert-butyldiphenylsiloxy)-4-dibenzylamino-3-hydroxy-N-methoxy-N-methylpentanamide
CAS No.:290354-72-2
Molecular Formula:C₄₄H₅₂N₂O₅Si
Molecular Weight:716.993
Hs Code.:

Synonyms:(2S,3R,4R)-2-Benzyloxy-5-(tert-butyldiphenylsiloxy)-4-dibenzylamino-3-hydroxy-N-methoxy-N-methylpentanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,4R)-2-Benzyloxy-5-(tert-butyldiphenylsiloxy)-4-dibenzylamino-3-hydroxy-N-methoxy-N-methylpentanamide

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Technology Process of (2S,3R,4R)-2-Benzyloxy-5-(tert-butyldiphenylsiloxy)-4-dibenzylamino-3-hydroxy-N-methoxy-N-methylpentanamide

There total 11 articles about (2S,3R,4R)-2-Benzyloxy-5-(tert-butyldiphenylsiloxy)-4-dibenzylamino-3-hydroxy-N-methoxy-N-methylpentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 290354-71-1
(2'S,3'R,4S,4'R)-4-Benzyl-3-[2'-benzyloxy-5'-(tert-butyldiphenylsiloxy)-4'-dibenzylamino-3'-hydroxypentanoyl]oxazolidin-2-one

: 290354-72-2
(2S,3R,4R)-2-Benzyloxy-5-(tert-butyldiphenylsiloxy)-4-dibenzylamino-3-hydroxy-N-methoxy-N-methylpentanamide

Guidance literature:: N,O-dimethylhydroxylamine*hydrochloride; With trimethylaluminum; In tetrahydrofuran; at -30 ℃;

(2'S,3'R,4S,4'R)-4-Benzyl-3-[2'-benzyloxy-5'-(tert-butyldiphenylsiloxy)-4'-dibenzylamino-3'-hydroxypentanoyl]oxazolidin-2-one; In tetrahydrofuran; at 0 ℃; for 2.5h;
DOI:10.1016/j.tetlet.2003.08.030

Reference yield: 93.0%

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 627859-97-6
(R)-4-Benzyl-3-[(2S,3R,4R)-2-benzyloxy-5-(tert-butyl-diphenyl-silanyloxy)-4-dibenzylamino-3-hydroxy-pentanoyl]-oxazolidin-2-one

: 290354-72-2
(2S,3R,4R)-2-Benzyloxy-5-(tert-butyldiphenylsiloxy)-4-dibenzylamino-3-hydroxy-N-methoxy-N-methylpentanamide

Guidance literature:: N,O-dimethylhydroxylamine*hydrochloride; With trimethylaluminum; In tetrahydrofuran; at -30 ℃;

(R)-4-Benzyl-3-[(2S,3R,4R)-2-benzyloxy-5-(tert-butyl-diphenyl-silanyloxy)-4-dibenzylamino-3-hydroxy-pentanoyl]-oxazolidin-2-one; In tetrahydrofuran; at -30 - 0 ℃; for 24h;
DOI:10.1016/j.tetlet.2003.08.030

Reference yield: 91.0%

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 627859-92-1
(2S,3R,4R)-2-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxy)-4-dibenzylamino-3-hydroxy-pentanoic acid methyl ester

: 290354-72-2
(2S,3R,4R)-2-Benzyloxy-5-(tert-butyldiphenylsiloxy)-4-dibenzylamino-3-hydroxy-N-methoxy-N-methylpentanamide

Guidance literature:: N,O-dimethylhydroxylamine*hydrochloride; With trimethylaluminum; In tetrahydrofuran; at -30 ℃;

(2S,3R,4R)-2-Benzyloxy-5-(tert-butyl-diphenyl-silanyloxy)-4-dibenzylamino-3-hydroxy-pentanoic acid methyl ester; In tetrahydrofuran; at -30 - 20 ℃; for 18h;
DOI:10.1016/j.tetlet.2003.08.030