D-Galactitol, 1,5-anhydro-1-C-(1,3-diphenyl-2-imidazolidinyl)-2,3,4-tris-O-(phenylmethyl)-6-O-(triphenylmethyl)-, (1S)-

Base Information

Chemical Name:D-Galactitol, 1,5-anhydro-1-C-(1,3-diphenyl-2-imidazolidinyl)-2,3,4-tris-O-(phenylmethyl)-6-O-(triphenylmethyl)-, (1S)-
CAS No.:228115-89-7
Molecular Formula:C61H58 N2 O5
Molecular Weight:0
Hs Code.:

Synonyms:D-Galactitol, 1,5-anhydro-1-C-(1,3-diphenyl-2-imidazolidinyl)-2,3,4-tris-O-(phenylmethyl)-6-O-(triphenylmethyl)-, (1S)-

Suppliers and Price of D-Galactitol, 1,5-anhydro-1-C-(1,3-diphenyl-2-imidazolidinyl)-2,3,4-tris-O-(phenylmethyl)-6-O-(triphenylmethyl)-, (1S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of D-Galactitol, 1,5-anhydro-1-C-(1,3-diphenyl-2-imidazolidinyl)-2,3,4-tris-O-(phenylmethyl)-6-O-(triphenylmethyl)-, (1S)-

Chemical Property:

PSA：52.63000
LogP:12.00160

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of D-Galactitol, 1,5-anhydro-1-C-(1,3-diphenyl-2-imidazolidinyl)-2,3,4-tris-O-(phenylmethyl)-6-O-(triphenylmethyl)-, (1S)-

There total 5 articles about D-Galactitol, 1,5-anhydro-1-C-(1,3-diphenyl-2-imidazolidinyl)-2,3,4-tris-O-(phenylmethyl)-6-O-(triphenylmethyl)-, (1S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 100-39-0
benzyl bromide

: 228115-88-6
1,3-diphenyl-2-(6-O-triphenylmethyl-β-D-galactopyranosyl)-imidazolidine

: 228115-89-7
1,3-diphenyl-2-(2,3,4-tri-O-benzyl-6-O-triphenylmethyl-β-D-galactopyranosyl)-imidazolidine

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/S0040-4020(99)00327-0

Reference yield:

: 52443-07-9
3,4,5,7-tetra-O-acetyl-2,6-anhydro-D-glycero-L-manno-heptonitrile

: 228115-89-7
1,3-diphenyl-2-(2,3,4-tri-O-benzyl-6-O-triphenylmethyl-β-D-galactopyranosyl)-imidazolidine

Guidance literature:: Multi-step reaction with 4 steps

1: NaH₂PO₂ / Raney nickel

2: sodium methoxide / methanol / 3 h

3: 1.93 g / triethylamine / CH₂Cl₂

4: 92 percent / sodium hydride / dimethylformamide / 0 - 20 °C

With sodium hypophosphite; sodium methylate; sodium hydride; triethylamine; nickel; In methanol; dichloromethane; N,N-dimethyl-formamide; 1: Reduction / 2: Deacetylation / 3: Etherification / 4: Alkylation;
DOI:10.1016/S0040-4020(99)00327-0

Reference yield:

: 76-83-5
trityl chloride

: 228115-89-7
1,3-diphenyl-2-(2,3,4-tri-O-benzyl-6-O-triphenylmethyl-β-D-galactopyranosyl)-imidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.93 g / triethylamine / CH₂Cl₂

2: 92 percent / sodium hydride / dimethylformamide / 0 - 20 °C

With sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide; 1: Etherification / 2: Alkylation;
DOI:10.1016/S0040-4020(99)00327-0