.beta.-D-Galactopyranose, 1,6-anhydro-2-O-(1,1-dimethylethyl)dimethylsilyl-3-O-(4-methoxyphenyl)methyl-

Base Information

Chemical Name:.beta.-D-Galactopyranose, 1,6-anhydro-2-O-(1,1-dimethylethyl)dimethylsilyl-3-O-(4-methoxyphenyl)methyl-
CAS No.:228115-71-7
Molecular Formula:C20H32 O6 Si
Molecular Weight:396.56
Hs Code.:

Synonyms:.beta.-D-Galactopyranose, 1,6-anhydro-2-O-(1,1-dimethylethyl)dimethylsilyl-3-O-(4-methoxyphenyl)methyl-

Suppliers and Price of .beta.-D-Galactopyranose, 1,6-anhydro-2-O-(1,1-dimethylethyl)dimethylsilyl-3-O-(4-methoxyphenyl)methyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of .beta.-D-Galactopyranose, 1,6-anhydro-2-O-(1,1-dimethylethyl)dimethylsilyl-3-O-(4-methoxyphenyl)methyl-

Chemical Property:

PSA：66.38000
LogP:3.08680

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of .beta.-D-Galactopyranose, 1,6-anhydro-2-O-(1,1-dimethylethyl)dimethylsilyl-3-O-(4-methoxyphenyl)methyl-

There total 3 articles about .beta.-D-Galactopyranose, 1,6-anhydro-2-O-(1,1-dimethylethyl)dimethylsilyl-3-O-(4-methoxyphenyl)methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 228115-62-6
1,6-anhydro-2-O-tert-butyldimethylsilyl-endo-3,4-O-p-methoxybenzylidene-β-D-galactopyranose

: 228115-71-7
1,6-anhydro-2-O-tert-butyldimethylsilyl-3-O-p-methoxybenzyl-β-D-galactopyranose

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; for 2h; Heating;
DOI:10.1016/S0040-4020(99)00327-0

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 228115-71-7
1,6-anhydro-2-O-tert-butyldimethylsilyl-3-O-p-methoxybenzyl-β-D-galactopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide

2: 56 percent / lithium aluminum hydride; aluminum chloride / tetrahydrofuran / 2 h / Heating

With 1H-imidazole; lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; N,N-dimethyl-formamide; 1: silylation / 2: Reduction;
DOI:10.1016/S0040-4020(99)00327-0

Reference yield:

: 228115-59-1
(1R,2S,6R,7R,8R)-4-(4-Methoxy-phenyl)-3,5,9,11-tetraoxa-tricyclo[6.2.1.0^2,6]undecan-7-ol

: 228115-71-7
1,6-anhydro-2-O-tert-butyldimethylsilyl-3-O-p-methoxybenzyl-β-D-galactopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide

2: 56 percent / lithium aluminum hydride; aluminum chloride / tetrahydrofuran / 2 h / Heating

With 1H-imidazole; lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; N,N-dimethyl-formamide; 1: silylation / 2: Reduction;
DOI:10.1016/S0040-4020(99)00327-0