phenyl-acetic acid 4-[{5-[2-(pyridin-2-yldisulfanyl)-ethylcarbamoyl]-pentylcarbamoyl}-(quinolin-6-ylcarbamoyloxy)-methyl]-phenyl ester

Base Information

Chemical Name:phenyl-acetic acid 4-[{5-[2-(pyridin-2-yldisulfanyl)-ethylcarbamoyl]-pentylcarbamoyl}-(quinolin-6-ylcarbamoyloxy)-methyl]-phenyl ester
CAS No.:697226-55-4
Molecular Formula:C₃₉H₃₉N₅O₆S₂
Molecular Weight:737.901
Hs Code.:

Synonyms:phenyl-acetic acid 4-[{5-[2-(pyridin-2-yldisulfanyl)-ethylcarbamoyl]-pentylcarbamoyl}-(quinolin-6-ylcarbamoyloxy)-methyl]-phenyl ester

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Chemical Property of phenyl-acetic acid 4-[{5-[2-(pyridin-2-yldisulfanyl)-ethylcarbamoyl]-pentylcarbamoyl}-(quinolin-6-ylcarbamoyloxy)-methyl]-phenyl ester

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Technology Process of phenyl-acetic acid 4-[{5-[2-(pyridin-2-yldisulfanyl)-ethylcarbamoyl]-pentylcarbamoyl}-(quinolin-6-ylcarbamoyloxy)-methyl]-phenyl ester

There total 9 articles about phenyl-acetic acid 4-[{5-[2-(pyridin-2-yldisulfanyl)-ethylcarbamoyl]-pentylcarbamoyl}-(quinolin-6-ylcarbamoyloxy)-methyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 580-15-4
6-aminoquinoline

: 697226-55-4
phenyl-acetic acid 4-[{5-[2-(pyridin-2-yldisulfanyl)-ethylcarbamoyl]-pentylcarbamoyl}-(quinolin-6-ylcarbamoyloxy)-methyl]-phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: Pd(PPh₃)4; acetic acid; N-methylalanine

2: EDC; DMAP

3: CF₃COOH

4: EDC

5: N-ethylmorpholine / dimethylformamide

With N-ethylmorpholine;; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-methylalanine; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1002/anie.200353204

Reference yield:

: 1198-84-1
4-hydroxymandelic acid

: 697226-55-4
phenyl-acetic acid 4-[{5-[2-(pyridin-2-yldisulfanyl)-ethylcarbamoyl]-pentylcarbamoyl}-(quinolin-6-ylcarbamoyloxy)-methyl]-phenyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: Cs₂CO₃

2: iPr₂NEt

3: Pd(PPh₃)4; acetic acid; N-methylalanine

4: EDC; DMAP

5: CF₃COOH

6: EDC

7: N-ethylmorpholine / dimethylformamide

With N-ethylmorpholine;; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-methylalanine; caesium carbonate; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1002/anie.200353204

Reference yield:

: 5514-98-7
6-aminohexanoic acid tert-butyl ester

: 697226-55-4
phenyl-acetic acid 4-[{5-[2-(pyridin-2-yldisulfanyl)-ethylcarbamoyl]-pentylcarbamoyl}-(quinolin-6-ylcarbamoyloxy)-methyl]-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: EDC; DMAP

2: CF₃COOH

3: EDC

4: N-ethylmorpholine / dimethylformamide

With N-ethylmorpholine;; dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1002/anie.200353204