N'-(3-methyl-4-oxo-1,4-dihydronaphthalen-1-ylidene)-1-(2,5-dimethylphenyl)-5-oxopyrrolidine-3-carbohydrazide

Base Information

Chemical Name:N'-(3-methyl-4-oxo-1,4-dihydronaphthalen-1-ylidene)-1-(2,5-dimethylphenyl)-5-oxopyrrolidine-3-carbohydrazide
CAS No.:1342800-30-9
Molecular Formula:C₂₄H₂₃N₃O₃
Molecular Weight:401.465
Hs Code.:

Synonyms:N'-(3-methyl-4-oxo-1,4-dihydronaphthalen-1-ylidene)-1-(2,5-dimethylphenyl)-5-oxopyrrolidine-3-carbohydrazide

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Chemical Property of N'-(3-methyl-4-oxo-1,4-dihydronaphthalen-1-ylidene)-1-(2,5-dimethylphenyl)-5-oxopyrrolidine-3-carbohydrazide

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Technology Process of N'-(3-methyl-4-oxo-1,4-dihydronaphthalen-1-ylidene)-1-(2,5-dimethylphenyl)-5-oxopyrrolidine-3-carbohydrazide

There total 2 articles about N'-(3-methyl-4-oxo-1,4-dihydronaphthalen-1-ylidene)-1-(2,5-dimethylphenyl)-5-oxopyrrolidine-3-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 956593-15-0
C₁₃H₁₇N₃O₂

: 58-27-5,34524-96-4
menadione

: 1342800-30-9
N'-(3-methyl-4-oxo-1,4-dihydronaphthalen-1-ylidene)-1-(2,5-dimethylphenyl)-5-oxopyrrolidine-3-carbohydrazide

Guidance literature:: With hydrogenchloride; In water; isopropyl alcohol; for 19h; Reflux;
DOI:10.1007/s11164-011-0306-y

Reference yield:

: methyl 1-(2,5-dimethylphenyl)-5-oxo-3-pyrrolidinecarboxylate

: 1342800-30-9
N'-(3-methyl-4-oxo-1,4-dihydronaphthalen-1-ylidene)-1-(2,5-dimethylphenyl)-5-oxopyrrolidine-3-carbohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / isopropyl alcohol / Reflux

2: hydrogenchloride / water; isopropyl alcohol / 19 h / Reflux

With hydrogenchloride; hydrazine hydrate; In water; isopropyl alcohol;
DOI:10.1007/s11164-011-0306-y

Reference yield: 84.0%

: 1342800-30-9
N'-(3-methyl-4-oxo-1,4-dihydronaphthalen-1-ylidene)-1-(2,5-dimethylphenyl)-5-oxopyrrolidine-3-carbohydrazide

: 75-03-6
ethyl iodide

: 1342800-37-6
N-ethyl-N'-(3-methyl-4-oxo-1,4-dihydronaphthalen-1-yl)-1-(2,5-dimethylphenyl)-5-oxopyrrolidine-3-carbohydrazide

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; In butanone; at 50 - 55 ℃; for 20h;
DOI:10.1007/s11164-011-0306-y