(μ-SCH2)2N(CH2C6H5)[Fe2(CO)4(tris(N-pyrrolyl)phosphine)2]

Base Information

Chemical Name:(μ-SCH2)2N(CH2C6H5)[Fe2(CO)4(tris(N-pyrrolyl)phosphine)2]
CAS No.:1021186-13-9
Molecular Formula:C₃₇H₃₅Fe₂N₇O₄P₂S₂
Molecular Weight:879.503
Hs Code.:

Synonyms:(μ-SCH2)2N(CH2C6H5)[Fe2(CO)4(tris(N-pyrrolyl)phosphine)2]

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Chemical Property of (μ-SCH2)2N(CH2C6H5)[Fe2(CO)4(tris(N-pyrrolyl)phosphine)2]

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Technology Process of (μ-SCH2)2N(CH2C6H5)[Fe2(CO)4(tris(N-pyrrolyl)phosphine)2]

There total 1 articles about (μ-SCH2)2N(CH2C6H5)[Fe2(CO)4(tris(N-pyrrolyl)phosphine)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 60259-30-5
tri-1-pyrrolylphosphine

: 1021186-12-8
{(μ-SCH₂)₂NCH₂C₆H₅}Fe₂(CO)₅P(Pyr)₃

: 1021186-13-9
(μ-SCH2)2N(CH2C6H5)[Fe2(CO)4(tris(N-pyrrolyl)phosphine)2]

Guidance literature:: In toluene; (under N2, Schlenk); ligand added to soln. of Fe-complex in toluene, refluxed for 20 h; solvent evapd. under reduced pressure, silica gel column chromy. with hexane/CH2Cl2 (4:1), then hexane/CH2Cl2 (3:1); elem. anal.;
DOI:10.1021/ic702010w

Reference yield:

: 1021186-13-9
(μ-SCH2)2N(CH2C6H5)[Fe2(CO)4(tris(N-pyrrolyl)phosphine)2]

: 1333-74-0
hydrogen

Guidance literature:: With ascorbic acid; In water; acetonitrile; Irradiation (UV/VIS); (under N2, Schlenk); Ru-complex, ascorbic acid, Fe-complex and MeCN added to tube, H2O added, stirred for 15 min, warmed to room temp., irradiated at 25°C with Xe lamp (500 W) for 3 h;
DOI:10.1021/ic702010w

Reference yield:

: 1021186-13-9
(μ-SCH2)2N(CH2C6H5)[Fe2(CO)4(tris(N-pyrrolyl)phosphine)2]

: (μ-SCH2)2N(CH2C6H5)[Fe2(CO)4(tris(N-pyrrolyl)phosphine)2](1-)

Guidance literature:: With tris(2,2’-bipyridine)ruthenium(II); In acetonitrile; Irradiation (UV/VIS); (under N2, Schlenk); soln. of Fe-complex in MeCN reacted with Ru-complexunder flash photolysis; monitored by UV/VIS; Kinetics;
DOI:10.1021/ic702010w