3-(1-methylindol-3-yl)-4-[1-(2-deoxy-3,4-di-O-p-toluyl-β-D-ribofuranosyl)indol-3-yl]furan-2,5-dione

Base Information

Chemical Name:3-(1-methylindol-3-yl)-4-[1-(2-deoxy-3,4-di-O-p-toluyl-β-D-ribofuranosyl)indol-3-yl]furan-2,5-dione
CAS No.:609843-63-2
Molecular Formula:C₄₂H₃₄N₂O₈
Molecular Weight:694.741
Hs Code.:

Synonyms:3-(1-methylindol-3-yl)-4-[1-(2-deoxy-3,4-di-O-p-toluyl-β-D-ribofuranosyl)indol-3-yl]furan-2,5-dione

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Chemical Property of 3-(1-methylindol-3-yl)-4-[1-(2-deoxy-3,4-di-O-p-toluyl-β-D-ribofuranosyl)indol-3-yl]furan-2,5-dione

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Technology Process of 3-(1-methylindol-3-yl)-4-[1-(2-deoxy-3,4-di-O-p-toluyl-β-D-ribofuranosyl)indol-3-yl]furan-2,5-dione

There total 3 articles about 3-(1-methylindol-3-yl)-4-[1-(2-deoxy-3,4-di-O-p-toluyl-β-D-ribofuranosyl)indol-3-yl]furan-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 118452-10-1
1-(2-deoxy-3,5-di-O-p-toluyl-β-D-ribofuranosyl)indole

: 79-37-8
oxalyl dichloride

: 1912-48-7
2-(1-methyl-1H-indol-3-yl)acetic acid

: 609843-63-2
3-(1-methylindol-3-yl)-4-[1-(2-deoxy-3,4-di-O-p-toluyl-β-D-ribofuranosyl)indol-3-yl]furan-2,5-dione

Guidance literature:: 1-(2-deoxy-3,5-di-O-p-toluyl-β-D-ribofuranosyl)indole; oxalyl dichloride; With silver carbonate; In dichloromethane; at 0 ℃; for 0.666667h;

2-(1-methyl-1H-indol-3-yl)acetic acid; With triethylamine; In dichloromethane; for 4h; Heating;
DOI:10.1023/A:1023212532748

Reference yield:

: 120-72-9
indole

: 609843-63-2
3-(1-methylindol-3-yl)-4-[1-(2-deoxy-3,4-di-O-p-toluyl-β-D-ribofuranosyl)indol-3-yl]furan-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: 54 percent / sodium hydride / various solvent(s); acetonitrile / 24 h / 20 °C

2.1: silver carbonate / CH₂Cl₂ / 0.67 h / 0 °C

2.2: 53 percent / triethylamine / CH₂Cl₂ / 4 h / Heating

With sodium hydride; silver carbonate; In dichloromethane; acetonitrile;
DOI:10.1023/A:1023212532748

Reference yield:

: 4330-21-6
2-deoxy-3,5-di-O-p-toluoyl-α-D-erythro-pentofuranosyl chloride

: 609843-63-2
3-(1-methylindol-3-yl)-4-[1-(2-deoxy-3,4-di-O-p-toluyl-β-D-ribofuranosyl)indol-3-yl]furan-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1.1: 54 percent / sodium hydride / various solvent(s); acetonitrile / 24 h / 20 °C

2.1: silver carbonate / CH₂Cl₂ / 0.67 h / 0 °C

2.2: 53 percent / triethylamine / CH₂Cl₂ / 4 h / Heating

With sodium hydride; silver carbonate; In dichloromethane; acetonitrile;
DOI:10.1023/A:1023212532748