Technology Process of C15H20O4
There total 1 articles about C15H20O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxygen; copper diacetate;
palladium dichloride;
In
N,N-dimethyl acetamide; water;
for 12h;
DOI:10.1021/ol070517g
- Guidance literature:
-
C15H20O4;
With
di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine;
In
diethyl ether; dichloromethane;
at -78 - -50 ℃;
(R,E)-5-(((tert-butyl)diphenylsilyl)oxy)-2,4-dimethylpent-2-enal;
In
diethyl ether; dichloromethane;
at -78 - -50 ℃;
for 6h;
With
dihydrogen peroxide;
In
various solvents;
pH=7;
Further stages.;
DOI:10.1021/ol070517g
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ethyldiisopropylamine; dibutylboron triflate / CH2Cl2; diethyl ether / -78 - -50 °C
1.2: CH2Cl2; diethyl ether / 6 h / -78 - -50 °C
1.3: 72 percent / aq. H2O2 / various solvents / pH 7
2.1: diethyl(methoxy)borane; NaBH4 / tetrahydrofuran; methanol / -78 °C
2.2: 85 percent / methanol
3.1: 81 percent / ethyldiisopropylamine / CHCl3 / 12 h / 65 °C
With
sodium tetrahydroborate; di-n-butylboryl trifluoromethanesulfonate; diethyl methoxy borane; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform;
1.2: Evans aldol reaction;
DOI:10.1021/ol070517g