Cyclohexene, 1-(3-methoxy-1-propynyl)- (9CI)

Base Information

Chemical Name:Cyclohexene, 1-(3-methoxy-1-propynyl)- (9CI)
CAS No.:227006-86-2
Molecular Formula:C10H14 O
Molecular Weight:150.21756
Hs Code.:
Mol file:227006-86-2.mol

Synonyms:Cyclohexene,1-(3-methoxy-1-propynyl)- (9CI)

Suppliers and Price of Cyclohexene, 1-(3-methoxy-1-propynyl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Cyclohexene, 1-(3-methoxy-1-propynyl)- (9CI)

Chemical Property:

PSA：9.23000
LogP:2.13660

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Cyclohexene, 1-(3-methoxy-1-propynyl)- (9CI)

There total 1 articles about Cyclohexene, 1-(3-methoxy-1-propynyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 931-49-7
1-ethenylcyclohexene

: 107-30-2
chloromethyl methyl ether

: 227006-86-2
1-(3-methoxy-2-propenyl)cyclohexene

Guidance literature:: 1-ethenylcyclohexene; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

chloromethyl methyl ether; at 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/acs.joc.9b02628

Reference yield: 72.0%

: 100-58-3
phenylmagnesium bromide

: 227006-86-2
1-(3-methoxy-2-propenyl)cyclohexene

: (1-(cyclohex-1-en-1-yl)propa-1,2-dien-1-yl)benzene

Guidance literature:: With copper(I) bromide; In diethyl ether; at -30 - 20 ℃; for 15h; Inert atmosphere;
DOI:10.1021/acs.joc.9b02628

Reference yield:

: 201230-82-2
carbon monoxide

: 227006-86-2
1-(3-methoxy-2-propenyl)cyclohexene

: (E)-2-Cyclohex-1-enyl-4-methoxy-but-2-enal

: 2-cyclohex-1-enyl-4-methoxy-butyraldehyde

: (E)-3-Cyclohex-1-enyl-2-methoxymethyl-propenal

Guidance literature:: With triphenyl phosphite; Rh(1+)(1,5-cyclooctadiene)(η6-C6H5B(1-)Ph3); hydrogen; In dichloromethane; at 60 ℃; for 48h; under 9120 Torr; Yield given; Yields of byproduct given;
DOI:10.1021/jo982425y