1,1-diphenyl-2-o-tolylethane-1,2-diol

Base Information

Chemical Name:1,1-diphenyl-2-o-tolylethane-1,2-diol
CAS No.:110247-81-9
Molecular Formula:C₂₁H₂₀O₂
Molecular Weight:304.389
Hs Code.:

Synonyms:1,1-diphenyl-2-o-tolylethane-1,2-diol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-diphenyl-2-o-tolylethane-1,2-diol

Chemical Property:

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Technology Process of 1,1-diphenyl-2-o-tolylethane-1,2-diol

There total 10 articles about 1,1-diphenyl-2-o-tolylethane-1,2-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 119-61-9
benzophenone

: 529-20-4
2-methylphenyl aldehyde

: 110247-81-9
1,1-diphenyl-2-o-tolylethane-1,2-diol

Guidance literature:: benzophenone; 2-methylphenyl aldehyde; With 1,3-bis(mesityl)imidazolium chloride; dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane; copper(l) chloride; sodium t-butanolate; In tetrahydrofuran; at 80 ℃; for 6h; Inert atmosphere; Sealed tube;

With hydrogenchloride; In tetrahydrofuran; water;
DOI:10.1021/jacs.8b13309

Reference yield:

: 932-31-0
ortho-tolylmagnesium bromide

: 110247-81-9
1,1-diphenyl-2-o-tolylethane-1,2-diol

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: LiAlH₄

With lithium aluminium tetrahydride; diethyl ether;
DOI:10.1021/ja01598a037

Reference yield:

: 134-81-6
benzil

: 110247-81-9
1,1-diphenyl-2-o-tolylethane-1,2-diol

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: LiAlH₄

With lithium aluminium tetrahydride; diethyl ether;
DOI:10.1021/ja01598a037