(4RS)-6-[3-butenyl(phenylsulfonyl)amino]-5-iodo-4-iodomethyl-7-methoxy-1-phenylsulfonyl-1,2,3,4-tetrahydroquinoline

Base Information

Chemical Name:(4RS)-6-[3-butenyl(phenylsulfonyl)amino]-5-iodo-4-iodomethyl-7-methoxy-1-phenylsulfonyl-1,2,3,4-tetrahydroquinoline
CAS No.:608537-12-8
Molecular Formula:C₂₇H₂₈I₂N₂O₅S₂
Molecular Weight:778.471
Hs Code.:

Synonyms:(4RS)-6-[3-butenyl(phenylsulfonyl)amino]-5-iodo-4-iodomethyl-7-methoxy-1-phenylsulfonyl-1,2,3,4-tetrahydroquinoline

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Chemical Property of (4RS)-6-[3-butenyl(phenylsulfonyl)amino]-5-iodo-4-iodomethyl-7-methoxy-1-phenylsulfonyl-1,2,3,4-tetrahydroquinoline

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Technology Process of (4RS)-6-[3-butenyl(phenylsulfonyl)amino]-5-iodo-4-iodomethyl-7-methoxy-1-phenylsulfonyl-1,2,3,4-tetrahydroquinoline

There total 11 articles about (4RS)-6-[3-butenyl(phenylsulfonyl)amino]-5-iodo-4-iodomethyl-7-methoxy-1-phenylsulfonyl-1,2,3,4-tetrahydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 608537-11-7
2-bromo-N¹,N⁴-bis(3-butenyl)-5-methoxy-N¹,N⁴-bis(phenylsulfonyl)-1,4-phenylenediamine

: (4RS)-6-[3-butenyl(phenylsulfonyl)amino]-5-iodo-7-methoxy-4-methyl-1-phenylsulfonyl-1,2,3,4-tetrahydroquinoline

: 608537-12-8
(4RS)-6-[3-butenyl(phenylsulfonyl)amino]-5-iodo-4-iodomethyl-7-methoxy-1-phenylsulfonyl-1,2,3,4-tetrahydroquinoline

Guidance literature:: 2-bromo-N¹,N⁴-bis(3-butenyl)-5-methoxy-N¹,N⁴-bis(phenylsulfonyl)-1,4-phenylenediamine; With zirconocene methyl chloride; tert.-butyl lithium; In tetrahydrofuran; hexane; at -78 - 40 ℃;

With iodine; In dichloromethane; at 20 ℃; for 14h; Further stages. Title compound not separated from byproducts.;
DOI:10.1002/ejoc.200300077

Reference yield: 34.0%

: 608537-15-1
2-bromo-N¹,N⁴-bis(3-butenyl)-6-methoxy-N¹,N⁴-bis(phenylsulfonyl)-1,4-phenylenediamine

: 608537-12-8
(4RS)-6-[3-butenyl(phenylsulfonyl)amino]-5-iodo-4-iodomethyl-7-methoxy-1-phenylsulfonyl-1,2,3,4-tetrahydroquinoline

Guidance literature:: 2-bromo-N¹,N⁴-bis(3-butenyl)-6-methoxy-N¹,N⁴-bis(phenylsulfonyl)-1,4-phenylenediamine; With zirconocene methyl chloride; tert.-butyl lithium; In tetrahydrofuran;

With iodine; In dichloromethane; Further stages.;
DOI:10.1002/ejoc.200300077