trioxobromo(2,2'-bipyridine)technetium(VII)

Base Information

• Chemical Name: trioxobromo(2,2'-bipyridine)technetium(VII)
• CAS No.: 78939-78-3
• Molecular Formula: C₁₀H₈BrN₂O₃Tc
• Molecular Weight: 381.996
• Mol file: 78939-78-3.mol

Synonyms:trioxobromo(2,2'-bipyridine)technetium(VII)

Chemical Property of trioxobromo(2,2'-bipyridine)technetium(VII)

Chemical Property:

Purity/Quality:

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Technology Process of trioxobromo(2,2'-bipyridine)technetium(VII)

There total 1 articles about trioxobromo(2,2'-bipyridine)technetium(VII) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

[2,2]bipyridinyl (366-18-7) + ammonium pertechnetate (34035-97-7) → trioxobromo(2,2'-bipyridine)technetium(VII) (78939-78-3)

Guidance literature:

With hydrogen bromide; In ethanol; soln. of ligand in EtOH added to stirred soln. of NH4TcO4 (molar ratio 7.6:1) in EtOH, 48% HBr added dropwise, stirred for 10 min; filtered, washed with 4 N HBr and acetone, dried in vac.; elem. anal.;

DOI:10.1021/ic50226a053

Reference yield:

trioxobromo(2,2'-bipyridine)technetium(VII) (78939-78-3) → pertechnetate anion (23288-61-1)

Guidance literature:

With water; In water; hydrolyzed in water;

DOI:10.1021/ic50226a053

upstream raw materials:

[2,2]bipyridinyl

ammonium pertechnetate

Downstream raw materials:

pertechnetate anion