5,10,15-tris(pentafluorophenyl)-20-(4,4,5,5-tetramethyl-[1,3]dioxaborolan-2-yl)por-phyrinatozinc(II)

Base Information

Chemical Name:5,10,15-tris(pentafluorophenyl)-20-(4,4,5,5-tetramethyl-[1,3]dioxaborolan-2-yl)por-phyrinatozinc(II)
CAS No.:1212020-74-0
Molecular Formula:C₄₄H₂₀BF₁₅N₄O₂Zn
Molecular Weight:997.845
Hs Code.:

Synonyms:5,10,15-tris(pentafluorophenyl)-20-(4,4,5,5-tetramethyl-[1,3]dioxaborolan-2-yl)por-phyrinatozinc(II)

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Chemical Property of 5,10,15-tris(pentafluorophenyl)-20-(4,4,5,5-tetramethyl-[1,3]dioxaborolan-2-yl)por-phyrinatozinc(II)

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Technology Process of 5,10,15-tris(pentafluorophenyl)-20-(4,4,5,5-tetramethyl-[1,3]dioxaborolan-2-yl)por-phyrinatozinc(II)

There total 2 articles about 5,10,15-tris(pentafluorophenyl)-20-(4,4,5,5-tetramethyl-[1,3]dioxaborolan-2-yl)por-phyrinatozinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 162479-06-3
5-bromo-10,15,20-tris(pentafluorophenyl)porphyrinatozinc(II)

: 73183-34-3
bis(pinacol)diborane

: 1212020-74-0
5,10,15-tris(pentafluorophenyl)-20-(4,4,5,5-tetramethyl-[1,3]dioxaborolan-2-yl)por-phyrinatozinc(II)

Guidance literature:: With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In N,N-dimethyl-formamide; at 80 ℃; for 4h; Inert atmosphere;

Reference yield: 66.0%

: 162479-06-3
5-bromo-10,15,20-tris(pentafluorophenyl)porphyrinatozinc(II)

: 73183-34-3
bis(pinacol)diborane

: 1212020-74-0
5,10,15-tris(pentafluorophenyl)-20-(4,4,5,5-tetramethyl-[1,3]dioxaborolan-2-yl)porphyrinatozinc(II)

Guidance literature:: With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium acetate; In N,N-dimethyl-formamide; at 80 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol902947h

Reference yield: 42.0%

: 1212020-74-0
5,10,15-tris(pentafluorophenyl)-20-(4,4,5,5-tetramethyl-[1,3]dioxaborolan-2-yl)por-phyrinatozinc(II)

: 352336-87-9
2,7-(1,1-dimethylethyl)-9,9-dimethyl-5-bromo-4-xanthenecarboxylic acid

: 5-[2,7-di-tert-butyl-5-hydroxycarbonyl-9,9-dimethylxanthen-4-yl]-10,15,20-tris(pentafluorophenyl)porphyrin

Guidance literature:: 5,10,15-tris(pentafluorophenyl)-20-(4,4,5,5-tetramethyl-[1,3]dioxaborolan-2-yl)por-phyrinatozinc(II); 2,7-(1,1-dimethylethyl)-9,9-dimethyl-5-bromo-4-xanthenecarboxylic acid; With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; toluene; at 90 ℃; for 18h; Inert atmosphere;

With hydrogenchloride; In dichloromethane; for 4h;