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Technology Process of (CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(1+)*GaCl4(1-)=(CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(GaCl4)

(CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(1+)*GaCl4(1-)=(CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(GaCl4)

Base Information
  • Chemical Name:(CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(1+)*GaCl4(1-)=(CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(GaCl4)
  • CAS No.:416900-98-6
  • Molecular Formula:C30H50N3P2Si*Cl4Ga
  • Molecular Weight:754.315
  • Hs Code.:
(CH<sub>3</sub>)3SiCP(N(CH(CH<sub>3</sub>)2)2)2NC(CH<sub>3</sub>)P(C<sub>6</sub>H<sub>5</sub>)2<sup>(1+)</sup>*GaCl<sub>4</sub><sup>(1-)</sup>=(CH<sub>3</sub>)3SiCP(N(CH(CH<sub>3</sub>)2)2)2NC(CH<sub>3</sub>)P(C<sub>6</sub>H<sub>5</sub>)2(GaCl<sub>4</sub>)

Synonyms:(CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(1+)*GaCl4(1-)=(CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(GaCl4)

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Chemical Property of (CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(1+)*GaCl4(1-)=(CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(GaCl4)
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Technology Process of (CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(1+)*GaCl4(1-)=(CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(GaCl4)

There total 1 articles about (CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(1+)*GaCl4(1-)=(CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(GaCl4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

Gallium trichloride
13450-90-3

Gallium trichloride

(((CH<sub>3</sub>)2CH)2N)2PClC(Si(CH<sub>3</sub>)3)P(C<sub>6</sub>H<sub>5</sub>)2
416900-96-4

(((CH3)2CH)2N)2PClC(Si(CH3)3)P(C6H5)2

(CH<sub>3</sub>)3SiCP(N(CH(CH<sub>3</sub>)2)2)2NC(CH<sub>3</sub>)P(C<sub>6</sub>H<sub>5</sub>)2<sup>(1+)</sup>*GaCl<sub>4</sub><sup>(1-)</sup>=(CH<sub>3</sub>)3SiCP(N(CH(CH<sub>3</sub>)2)2)2NC(CH<sub>3</sub>)P(C<sub>6</sub>H<sub>5</sub>)2(GaCl<sub>4</sub>)
416900-98-6

(CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(1+)*GaCl4(1-)=(CH3)3SiCP(N(CH(CH3)2)2)2NC(CH3)P(C6H5)2(GaCl4)

Guidance literature:
In dichloromethane; acetonitrile; under Ar atm. MeCN soln. GaCl3 was added to CH2Cl2 soln. ylide at -78°C, soln. was warmed slowly to room temp.; solvent was removed under vac.; residue was washed with Et2O, and recrystd. from CH2Cl2/Et2O;
DOI:10.1021/ja010347h
upstream raw materials:

Gallium trichloride

(((CH3)2CH)2N)2PClC(Si(CH3)3)P(C6H5)2

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