Diethyl 1-(2-cyclohexen-1-yl)-1,2-hydrazinedicarboxylate

Base Information

• Chemical Name: Diethyl 1-(2-cyclohexen-1-yl)-1,2-hydrazinedicarboxylate
• CAS No.: 17833-25-9
• Molecular Formula: C₁₂H₂₀N₂O₄
• Molecular Weight: 256.302
• Mol file: 17833-25-9.mol

Synonyms:Diethyl 1-(2-cyclohexen-1-yl)-1,2-hydrazinedicarboxylate

Chemical Property of Diethyl 1-(2-cyclohexen-1-yl)-1,2-hydrazinedicarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Diethyl 1-(2-cyclohexen-1-yl)-1,2-hydrazinedicarboxylate

There total 3 articles about Diethyl 1-(2-cyclohexen-1-yl)-1,2-hydrazinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

cyclohexene (110-83-8) + diethylazodicarboxylate (1972-28-7,218603-74-8) → Diethyl 1-(2-cyclohexen-1-yl)-1,2-hydrazinedicarboxylate (17833-25-9)

Guidance literature:

With tin(IV) chloride; In dichloromethane; at -78 ℃;

DOI:10.1021/ol902313v

Reference yield:

diethyl diazodicarboxylate (4143-61-7,218603-74-8) + cyclohexene (110-83-8) → Diethyl 1-(2-cyclohexen-1-yl)-1,2-hydrazinedicarboxylate (17833-25-9)

Guidance literature:

auch nach Zusatz von Radikalbildnern und Radikalfaengner;

Reference yield:

→ Diethyl 1-(2-cyclohexen-1-yl)-1,2-hydrazinedicarboxylate (17833-25-9)

Guidance literature:

Azodicarbonsaeure-diethylester, sd. Cyclohexen, Azo-bis-isobutyronitril;

DOI:10.1021/ja00863a017

upstream raw materials:

diethyl diazodicarboxylate

cyclohexene

diethylazodicarboxylate

Downstream raw materials:

C₁₅H₂₄N₂O₆

3-<(ethoxycarbonyl)amino>cyclohexene