benzoylamino methyl-2 (N-benzoylglycyloxy-2 cyclopentyloxy)-2 trimethylene-4,5 dioxolanne-1,3

Base Information

• Chemical Name: benzoylamino methyl-2 (N-benzoylglycyloxy-2 cyclopentyloxy)-2 trimethylene-4,5 dioxolanne-1,3
• CAS No.: 95778-26-0
• Molecular Formula: C₂₈H₃₂N₂O₇
• Molecular Weight: 508.571

Synonyms:benzoylamino methyl-2 (N-benzoylglycyloxy-2 cyclopentyloxy)-2 trimethylene-4,5 dioxolanne-1,3

Chemical Property of benzoylamino methyl-2 (N-benzoylglycyloxy-2 cyclopentyloxy)-2 trimethylene-4,5 dioxolanne-1,3

Chemical Property:

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Technology Process of benzoylamino methyl-2 (N-benzoylglycyloxy-2 cyclopentyloxy)-2 trimethylene-4,5 dioxolanne-1,3

There total 2 articles about benzoylamino methyl-2 (N-benzoylglycyloxy-2 cyclopentyloxy)-2 trimethylene-4,5 dioxolanne-1,3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

perchlorate de phenyl-2-oxazolinium-1,3,5 spiro-2' (trimethylene-4',5') dioxolanne-1',3' (62007-98-1) → benzoylamino methyl-2 (N-benzoylglycyloxy-2 cyclopentyloxy)-2 trimethylene-4,5 dioxolanne-1,3 (95778-26-0)

Guidance literature:

With TEA; water; In dichloromethane; for 0.166667h; Ambient temperature;

DOI:10.1016/S0040-4020(01)91488-7

Reference yield: 45.0%

N,N-dimethylammonium chloride (506-59-2) + perchlorate de phenyl-2-oxazolinium-1,3,5 spiro-2' (trimethylene-4',5') dioxolanne-1',3' (62007-98-1) → Benzoylamino-acetic acid 2-hydroxy-cyclopentyl ester (62007-93-6,91146-16-6) + benzoylamino methyl-2 (N-benzoylglycyloxy-2 cyclopentyloxy)-2 trimethylene-4,5 dioxolanne-1,3 (95778-26-0) + (benzoylamino) methyl-2 dimetylamino-2 trimethylene-4,5 dioxolanne-1,3 (95778-27-1) + (benzoylamino) methyl-2 dimetylamino-2 trimethylene-4,5 dioxolanne-1,3 (95778-27-1)

Guidance literature:

With triethylamine; In dichloromethane; for 0.166667h; Further byproducts given. Yields of byproduct given; Ambient temperature;

DOI:10.1016/S0040-4020(01)91488-7

Reference yield: 98.0%

benzoylamino methyl-2 (N-benzoylglycyloxy-2 cyclopentyloxy)-2 trimethylene-4,5 dioxolanne-1,3 (95778-26-0) → Benzoylamino-acetic acid 2-hydroxy-cyclopentyl ester (62007-93-6,91146-16-6)

Guidance literature:

With sulfuric acid; water; In dichloromethane;

DOI:10.1016/S0040-4020(01)91488-7

upstream raw materials:

N,N-dimethylammonium chloride

perchlorate de phenyl-2-oxazolinium-1,3,5 spiro-2' (trimethylene-4',5') dioxolanne-1',3'

Downstream raw materials:

Benzoylamino-acetic acid 2-hydroxy-cyclopentyl ester

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