S-(n-butyl) 4-methylbenzothioate

Base Information

• Chemical Name: S-(n-butyl) 4-methylbenzothioate
• CAS No.: 15676-93-4
• Molecular Formula: C₁₂H₁₆OS
• Molecular Weight: 208.324
• Mol file: 15676-93-4.mol

Synonyms:S-(n-butyl) 4-methylbenzothioate

Chemical Property of S-(n-butyl) 4-methylbenzothioate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of S-(n-butyl) 4-methylbenzothioate

There total 11 articles about S-(n-butyl) 4-methylbenzothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-bromo-butane (109-65-9) + 4-methyl-benzoyl chloride (874-60-2) → S-(n-butyl) 4-methylbenzothioate (15676-93-4)

Guidance literature:

With potassium carbonate; thiourea; In water; at 60 ℃; for 8h;

DOI:10.1002/adsc.201201059

Reference yield: 92.0%

n-butanethiol (109-79-5) + (4-methylphenyl)(oxo)acetic acid (7163-50-0) → S-(n-butyl) 4-methylbenzothioate (15676-93-4)

Guidance literature:

With dipotassium peroxodisulfate; In water; acetonitrile; at 70 ℃; for 24h; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1039/c5ob00769k

Reference yield: 88.0%

n-butanethiol (109-79-5) + 4-tolyl iodide (624-31-7) + chromium(0) hexacarbonyl (199620-14-9,13007-92-6) → S-(n-butyl) 4-methylbenzothioate (15676-93-4)

Guidance literature:

With potassium carbonate; nickel dichloride; In acetonitrile; at 70 ℃; for 1.5h;

DOI:10.1039/c5nj00655d

upstream raw materials:

butyl chlorothioformate

toluene

carbon monoxide

But-(E)-ylidene-(1-phenyl-ethyl)-amine