(ethoxycarbonyl)(cyano)(phenyl)methyl dimethyl phosphate

Base Information

• Chemical Name: (ethoxycarbonyl)(cyano)(phenyl)methyl dimethyl phosphate
• CAS No.: 952514-97-5
• Molecular Formula: C₁₃H₁₆NO₆P
• Molecular Weight: 313.247
• Mol file: 952514-97-5.mol

Synonyms:(ethoxycarbonyl)(cyano)(phenyl)methyl dimethyl phosphate

Chemical Property of (ethoxycarbonyl)(cyano)(phenyl)methyl dimethyl phosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of (ethoxycarbonyl)(cyano)(phenyl)methyl dimethyl phosphate

There total 1 articles about (ethoxycarbonyl)(cyano)(phenyl)methyl dimethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl benzoylphosphonate (18106-71-3) + potassium cyanide (151-50-8) + ethyl cyanoformate (623-49-4) → (ethoxycarbonyl)(cyano)(phenyl)methyl dimethyl phosphate (952514-97-5)

Guidance literature:

With 18-crown-6 ether; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jo0710073

Reference yield:

(ethoxycarbonyl)(cyano)(phenyl)methyl dimethyl phosphate (952514-97-5) → phenylglyoxylic acid ethyl ester (1603-79-8)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran;

DOI:10.1021/jo0710073

Reference yield:

(ethoxycarbonyl)(cyano)(phenyl)methyl dimethyl phosphate (952514-97-5) → ethyl (RS)-α-(aminomethyl)benzene acetate hydrochloride (29753-99-9)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; for 4h; under 3102.97 Torr;

DOI:10.1021/jo0710073

upstream raw materials:

dimethyl benzoylphosphonate

potassium cyanide

ethyl cyanoformate

Downstream raw materials:

ethyl (RS)-α-(aminomethyl)benzene acetate hydrochloride

phenylglyoxylic acid ethyl ester

ethyl 3-amino-2-hydroxy-2-phenylpropanoate